Technology Process of (1R,3S)-1,2,2-Trimethyl-3-<(triphenylmethoxy)methyl>cyclopentancarbaldehyd
There total 3 articles about (1R,3S)-1,2,2-Trimethyl-3-<(triphenylmethoxy)methyl>cyclopentancarbaldehyd which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
silica gel; pyridinium chlorochromate;
In
dichloromethane;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 66 percent / LiAlH4 / tetrahydrofuran / 12 h / Heating
2: 71 percent / 4-(dimethylamino)pyridine / pyridine / 12 h
3: 98 percent / pyridiniumchlorochromate, silica gel / CH2Cl2 / Ambient temperature
With
dmap; lithium aluminium tetrahydride; silica gel; pyridinium chlorochromate;
In
tetrahydrofuran; pyridine; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 71 percent / 4-(dimethylamino)pyridine / pyridine / 12 h
2: 98 percent / pyridiniumchlorochromate, silica gel / CH2Cl2 / Ambient temperature
With
dmap; silica gel; pyridinium chlorochromate;
In
pyridine; dichloromethane;