Technology Process of C18H13N3O3S
There total 6 articles about C18H13N3O3S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0); tris-(o-tolyl)phosphine / N,N-dimethyl-formamide / 80 °C
2: hydrogenchloride / methanol / 3 h / 20 °C
3: (1S,2S)-N,N'-dimethyl-1,2-diaminocyclohexane; copper(l) iodide; potassium phosphate; 1,3,5-trimethyl-benzene / 185 °C
4: sodium hydroxide / ethanol / 20 °C
With
hydrogenchloride; potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0); copper(l) iodide; (1S,2S)-N,N'-dimethyl-1,2-diaminocyclohexane; tris-(o-tolyl)phosphine; sodium hydroxide; 1,3,5-trimethyl-benzene;
In
methanol; ethanol; N,N-dimethyl-formamide;
1: |Suzuki-Miyaura Coupling / 3: |Buchwald Indole Synthesis;
DOI:10.1016/j.bmcl.2014.01.052
- Guidance literature:
-
Multi-step reaction with 3 steps
1: hydrogenchloride / methanol / 3 h / 20 °C
2: (1S,2S)-N,N'-dimethyl-1,2-diaminocyclohexane; copper(l) iodide; potassium phosphate; 1,3,5-trimethyl-benzene / 185 °C
3: sodium hydroxide / ethanol / 20 °C
With
hydrogenchloride; potassium phosphate; copper(l) iodide; (1S,2S)-N,N'-dimethyl-1,2-diaminocyclohexane; sodium hydroxide; 1,3,5-trimethyl-benzene;
In
methanol; ethanol;
2: |Buchwald Indole Synthesis;
DOI:10.1016/j.bmcl.2014.01.052
