4,5-bis-(N,N-diethylaminophenylphosphino)-2,7-di-tertbutyl-9,9-dimethylxanthene

Base Information

Chemical Name:4,5-bis-(N,N-diethylaminophenylphosphino)-2,7-di-tertbutyl-9,9-dimethylxanthene
CAS No.:1329609-26-8
Molecular Formula:C₄₃H₅₈N₂OP₂
Molecular Weight:680.894
Hs Code.:

Synonyms:4,5-bis-(N,N-diethylaminophenylphosphino)-2,7-di-tertbutyl-9,9-dimethylxanthene

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Chemical Property of 4,5-bis-(N,N-diethylaminophenylphosphino)-2,7-di-tertbutyl-9,9-dimethylxanthene

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Technology Process of 4,5-bis-(N,N-diethylaminophenylphosphino)-2,7-di-tertbutyl-9,9-dimethylxanthene

There total 1 articles about 4,5-bis-(N,N-diethylaminophenylphosphino)-2,7-di-tertbutyl-9,9-dimethylxanthene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 130525-43-8
4,5-dibromo-2,7-di-tert-butyl-9,9-dimethyl-9H-xanthene

: 4073-31-8
(diethylamino)phenylchlorophosphine

: 1329609-26-8
4,5-bis-(N,N-diethylaminophenylphosphino)-2,7-di-tertbutyl-9,9-dimethylxanthene

: 4,5-bis-(N,N-diethylaminophenylphosphino)-2,7-di-tertbutyl-9,9-dimethylxanthene

Guidance literature:: 4,5-dibromo-2,7-di-tert-butyl-9,9-dimethyl-9H-xanthene; With n-butyllithium; In diethyl ether; hexane; at -78 ℃; for 2h; Inert atmosphere;

(diethylamino)phenylchlorophosphine; In diethyl ether; hexane; at -78 - 20 ℃; optical yield given as %de; Inert atmosphere;
DOI:10.1016/j.jorganchem.2011.06.019