(6bR,6cS)-6c-(Diphenyl-phosphinoyl)-2-methoxy-2a,2b,6b,6c-tetrahydro-benzo[a]cyclopropa[cd]pentalene

Base Information

Chemical Name:(6bR,6cS)-6c-(Diphenyl-phosphinoyl)-2-methoxy-2a,2b,6b,6c-tetrahydro-benzo[a]cyclopropa[cd]pentalene
CAS No.:96617-99-1
Molecular Formula:C₂₅H₂₁O₂P
Molecular Weight:384.414
Hs Code.:

Synonyms:(6bR,6cS)-6c-(Diphenyl-phosphinoyl)-2-methoxy-2a,2b,6b,6c-tetrahydro-benzo[a]cyclopropa[cd]pentalene

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Chemical Property of (6bR,6cS)-6c-(Diphenyl-phosphinoyl)-2-methoxy-2a,2b,6b,6c-tetrahydro-benzo[a]cyclopropa[cd]pentalene

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Technology Process of (6bR,6cS)-6c-(Diphenyl-phosphinoyl)-2-methoxy-2a,2b,6b,6c-tetrahydro-benzo[a]cyclopropa[cd]pentalene

There total 4 articles about (6bR,6cS)-6c-(Diphenyl-phosphinoyl)-2-methoxy-2a,2b,6b,6c-tetrahydro-benzo[a]cyclopropa[cd]pentalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 96617-97-9
C₂₅H₂₁N₂O₂P

: 96617-99-1
(6bR,6cS)-6c-(Diphenyl-phosphinoyl)-2-methoxy-2a,2b,6b,6c-tetrahydro-benzo[a]cyclopropa[cd]pentalene

Guidance literature:: In xylene; at 135 ℃; for 0.25h;

Reference yield: 82.0%

: 96617-97-9
C₂₅H₂₁N₂O₂P

: 96617-99-1
6c-(Diphenyl-phosphinoyl)-2-methoxy-2a,2b,6b,6c-tetrahydro-benzo[a]cyclopropa[cd]pentalene

Guidance literature:: In xylene; for 0.25h; Heating;

Reference yield:

: 5353-66-2
diphenylphosphorylazide

: 96617-99-1
(6bR,6cS)-6c-(Diphenyl-phosphinoyl)-2-methoxy-2a,2b,6b,6c-tetrahydro-benzo[a]cyclopropa[cd]pentalene

Guidance literature:: Multi-step reaction with 3 steps

1: NEt₃ / CH₂Cl₂ / -15 - 0 °C

2: CH₂Cl₂ / 20 °C

3: 100 percent / xylene / 0.25 h / 135 °C

With triethylamine; In dichloromethane; xylene;