(4aS,5R,6S,8aR)-5-[(2,3,6-trimethoxyphenyl)(hydroxy)methyl]-5,6,8a-trimethyldecahydronaphthalene-1-spiro-2'-(1',3'-dioxolane)

Base Information

Chemical Name:(4aS,5R,6S,8aR)-5-[(2,3,6-trimethoxyphenyl)(hydroxy)methyl]-5,6,8a-trimethyldecahydronaphthalene-1-spiro-2'-(1',3'-dioxolane)
CAS No.:1070795-39-9
Molecular Formula:C₂₅H₃₈O₆
Molecular Weight:434.573
Hs Code.:

Synonyms:(4aS,5R,6S,8aR)-5-[(2,3,6-trimethoxyphenyl)(hydroxy)methyl]-5,6,8a-trimethyldecahydronaphthalene-1-spiro-2'-(1',3'-dioxolane)

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Chemical Property of (4aS,5R,6S,8aR)-5-[(2,3,6-trimethoxyphenyl)(hydroxy)methyl]-5,6,8a-trimethyldecahydronaphthalene-1-spiro-2'-(1',3'-dioxolane)

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Technology Process of (4aS,5R,6S,8aR)-5-[(2,3,6-trimethoxyphenyl)(hydroxy)methyl]-5,6,8a-trimethyldecahydronaphthalene-1-spiro-2'-(1',3'-dioxolane)

There total 1 articles about (4aS,5R,6S,8aR)-5-[(2,3,6-trimethoxyphenyl)(hydroxy)methyl]-5,6,8a-trimethyldecahydronaphthalene-1-spiro-2'-(1',3'-dioxolane) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: C₉H₁₁LiO₃

: 199180-19-3
cis-decaline

: 1070795-39-9
(4aS,5R,6S,8aR)-5-[(2,3,6-trimethoxyphenyl)(hydroxy)methyl]-5,6,8a-trimethyldecahydronaphthalene-1-spiro-2'-(1',3'-dioxolane)

Guidance literature:: DOI:10.1021/jo801404u

Reference yield: 92.0%

: 1070795-39-9
(4aS,5R,6S,8aR)-5-[(2,3,6-trimethoxyphenyl)(hydroxy)methyl]-5,6,8a-trimethyldecahydronaphthalene-1-spiro-2'-(1',3'-dioxolane)

: 1070795-41-3
(4aS,5R,6S,8aR)-5-[(2,3,6-trimethoxyphenyl)methyl]-5,6,8a-trimethyldecahydronaphthalene-1-spiro-2'-(1',3'-dioxolane)

Guidance literature:: (4aS,5R,6S,8aR)-5-[(2,3,6-trimethoxyphenyl)(hydroxy)methyl]-5,6,8a-trimethyldecahydronaphthalene-1-spiro-2'-(1',3'-dioxolane); With carbon disulfide; sodium hexamethyldisilazane; In tetrahydrofuran; at -78 - -55 ℃; for 1h;

With methyl iodide; In tetrahydrofuran; at -78 - -55 ℃; for 1h;

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; at 110 ℃; for 2h; Further stages.;
DOI:10.1021/jo801404u