Technology Process of C19H26N4O6
There total 7 articles about C19H26N4O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium methylate;
In
methanol;
at 20 ℃;
for 24h;
Inert atmosphere;
DOI:10.1002/chem.201003402
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: tetrabutylammomium bromide; palladium diacetate; sodium hydrogencarbonate / N,N-dimethyl-formamide / 8 h / 85 °C / Inert atmosphere
2.1: sodium methylate / methanol / 24 h / 20 °C
3.1: water; lithium hydroxide / tetrahydrofuran; methanol; water / 3 h / 20 °C / Inert atmosphere
4.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0 - 20 °C
4.2: 20 °C
5.1: sodium methylate / methanol / 24 h / 20 °C / Inert atmosphere
With
tetrabutylammomium bromide; water; sodium methylate; palladium diacetate; sodium hydrogencarbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; lithium hydroxide;
In
tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;
1.1: Heck coupling / 2.1: Zemplen reaction / 5.1: Zemplen reaction;
DOI:10.1002/chem.201003402
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium methylate / methanol / 24 h / 20 °C
2.1: water; lithium hydroxide / tetrahydrofuran; methanol; water / 3 h / 20 °C / Inert atmosphere
3.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0 - 20 °C
3.2: 20 °C
4.1: sodium methylate / methanol / 24 h / 20 °C / Inert atmosphere
With
water; sodium methylate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; lithium hydroxide;
In
tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;
1.1: Zemplen reaction / 4.1: Zemplen reaction;
DOI:10.1002/chem.201003402