Technology Process of C30H30N2O7S
There total 5 articles about C30H30N2O7S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium carbonate; triphenylphosphine / tetrakis(triphenylphosphine) palladium(0) / methanol; toluene / 80 °C / Inert atmosphere
2.1: hydrazine hydrate / palladium 10% on activated carbon / ethanol / 3 h / 80 °C
3.1: triethylamine / dmap / dichloromethane / 20 °C
4.1: sodium hydride / water; N,N-dimethyl-formamide / 0.17 h
4.2: 19 h / 20 °C
5.1: tris-(o-tolyl)phosphine; silver carbonate / palladium diacetate / N,N-dimethyl-formamide / Inert atmosphere
With
sodium hydride; sodium carbonate; hydrazine hydrate; triethylamine; triphenylphosphine; tris-(o-tolyl)phosphine; silver carbonate;
dmap; tetrakis(triphenylphosphine) palladium(0); palladium 10% on activated carbon; palladium diacetate;
In
methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium carbonate; triphenylphosphine / tetrakis(triphenylphosphine) palladium(0) / methanol; toluene / 80 °C / Inert atmosphere
2.1: hydrazine hydrate / palladium 10% on activated carbon / ethanol / 3 h / 80 °C
3.1: triethylamine / dmap / dichloromethane / 20 °C
4.1: sodium hydride / water; N,N-dimethyl-formamide / 0.17 h
4.2: 19 h / 20 °C
5.1: tris-(o-tolyl)phosphine; silver carbonate / palladium diacetate / N,N-dimethyl-formamide / Inert atmosphere
With
sodium hydride; sodium carbonate; hydrazine hydrate; triethylamine; triphenylphosphine; tris-(o-tolyl)phosphine; silver carbonate;
dmap; tetrakis(triphenylphosphine) palladium(0); palladium 10% on activated carbon; palladium diacetate;
In
methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: triethylamine / dmap / dichloromethane / 20 °C
2.1: sodium hydride / water; N,N-dimethyl-formamide / 0.17 h
2.2: 19 h / 20 °C
3.1: tris-(o-tolyl)phosphine; silver carbonate / palladium diacetate / N,N-dimethyl-formamide / Inert atmosphere
With
sodium hydride; triethylamine; tris-(o-tolyl)phosphine; silver carbonate;
dmap; palladium diacetate;
In
dichloromethane; water; N,N-dimethyl-formamide;