Technology Process of C24H28O5
There total 3 articles about C24H28O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide;
In
dichloromethane;
at 20 ℃;
for 2h;
Inert atmosphere;
Molecular sieve;
DOI:10.1021/ja200089f
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: 3,3-dimethyldioxirane / dichloromethane / -78 - 0 °C / Inert atmosphere
1.2: 1.17 h / -78 - 0 °C / Inert atmosphere
1.3: 0 °C
2.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 2 h / 20 °C / Inert atmosphere; Molecular sieve
With
tetrapropylammonium perruthennate; 3,3-dimethyldioxirane; 4-methylmorpholine N-oxide;
In
dichloromethane;
DOI:10.1021/ja200089f
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride
2.1: 3,3-dimethyldioxirane / dichloromethane / -78 - 0 °C / Inert atmosphere
2.2: 1.17 h / -78 - 0 °C / Inert atmosphere
2.3: 0 °C
3.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 2 h / 20 °C / Inert atmosphere; Molecular sieve
With
tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; tetrapropylammonium perruthennate; 3,3-dimethyldioxirane; 4-methylmorpholine N-oxide;
In
dichloromethane;
DOI:10.1021/ja200089f
