(2S)-ethoxy-3-(4-methoxyphenyl)propanoic acid (S)-1-(1-naphthyl)ethylamine salt

Base Information

Chemical Name:(2S)-ethoxy-3-(4-methoxyphenyl)propanoic acid (S)-1-(1-naphthyl)ethylamine salt
CAS No.:343880-42-2
Molecular Formula:C₁₂H₁₃N*C₁₂H₁₆O₄
Molecular Weight:395.499
Hs Code.:

Synonyms:(2S)-ethoxy-3-(4-methoxyphenyl)propanoic acid (S)-1-(1-naphthyl)ethylamine salt

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Chemical Property of (2S)-ethoxy-3-(4-methoxyphenyl)propanoic acid (S)-1-(1-naphthyl)ethylamine salt

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Technology Process of (2S)-ethoxy-3-(4-methoxyphenyl)propanoic acid (S)-1-(1-naphthyl)ethylamine salt

There total 4 articles about (2S)-ethoxy-3-(4-methoxyphenyl)propanoic acid (S)-1-(1-naphthyl)ethylamine salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 10420-89-0
(S)-1-(1-Naphthyl)ethylamine

: 2-ethoxy-3-(4-methoxyphenyl)propanoic acid

: 343880-41-1
(S)-2-ethoxy-3-(4-methoxyphenyl)propanoic acid

: 343880-42-2
(2S)-ethoxy-3-(4-methoxyphenyl)propanoic acid (S)-1-(1-naphthyl)ethylamine salt

Guidance literature:: In Isopropyl acetate; at 45 - 47 ℃; for 0.166667h;
DOI:10.1021/op040006z

Reference yield:

: ethyl 2-ethoxy-3-(4-methoxyphenyl)-2-propenoate

: 343880-42-2
(2S)-ethoxy-3-(4-methoxyphenyl)propanoic acid (S)-1-(1-naphthyl)ethylamine salt

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide; ethanol / toluene

2: hydrogen; 5%-palladium/activated carbon / Isopropyl acetate / 3 h / 22 - 25 °C / 3000.3 Torr / Autoclave; Inert atmosphere

3: Isopropyl acetate / 0.17 h / 45 - 47 °C

With ethanol; 5%-palladium/activated carbon; hydrogen; sodium hydroxide; In Isopropyl acetate; toluene;
DOI:10.1021/op040006z