ethyl 4-((2R,3R,4R,5S,6R)-2,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-3-ylamino)benzoate

Base Information

Chemical Name:ethyl 4-((2R,3R,4R,5S,6R)-2,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-3-ylamino)benzoate
CAS No.:1415608-28-4
Molecular Formula:C₄₃H₄₅NO₇
Molecular Weight:687.833
Hs Code.:

Synonyms:ethyl 4-((2R,3R,4R,5S,6R)-2,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-3-ylamino)benzoate

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Chemical Property of ethyl 4-((2R,3R,4R,5S,6R)-2,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-3-ylamino)benzoate

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Technology Process of ethyl 4-((2R,3R,4R,5S,6R)-2,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-3-ylamino)benzoate

There total 2 articles about ethyl 4-((2R,3R,4R,5S,6R)-2,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-3-ylamino)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: benzyl 2-amino-2-deoxy-3,4,6-tri-O-benzyl-β-D-glucopyranoside hydrochloride

: 51934-41-9
4-iodobenzoic acid ethyl ester

: 1415608-28-4
ethyl 4-((2R,3R,4R,5S,6R)-2,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-3-ylamino)benzoate

Guidance literature:: With copper(l) iodide; 2-acetylcyclohexanone; caesium carbonate; In N,N-dimethyl-formamide; at 130 ℃; Schlenk technique; Inert atmosphere; Sealed tube;
DOI:10.1016/j.tetlet.2012.10.069

Reference yield:

: 62098-37-7
benzyl 2-Amino-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranoside

: 4334-88-7
p-ethoxycarbonylphenylboronic acid

: 1415608-28-4
ethyl 4-((2R,3R,4R,5S,6R)-2,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-3-ylamino)benzoate

Guidance literature:: p-ethoxycarbonylphenylboronic acid; With copper diacetate; In dichloromethane; acetonitrile; at 20 ℃; for 0.166667h; Molecular sieve;

benzyl 2-Amino-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranoside; In dichloromethane; acetonitrile; at 65 ℃; for 24h; Molecular sieve;
DOI:10.1080/07328303.2013.816851