ethyl 2-{[5-anilino-2-(isopropylamino)phenyl]sulfanyl}acetate

Base Information

• Chemical Name: ethyl 2-{[5-anilino-2-(isopropylamino)phenyl]sulfanyl}acetate
• CAS No.: 371965-85-4
• Molecular Formula: C₁₉H₂₄N₂O₂S
• Molecular Weight: 344.478
• Mol file: 371965-85-4.mol

Synonyms:ethyl 2-{[5-anilino-2-(isopropylamino)phenyl]sulfanyl}acetate

Chemical Property of ethyl 2-{[5-anilino-2-(isopropylamino)phenyl]sulfanyl}acetate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of ethyl 2-{[5-anilino-2-(isopropylamino)phenyl]sulfanyl}acetate

There total 2 articles about ethyl 2-{[5-anilino-2-(isopropylamino)phenyl]sulfanyl}acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

N-[4-(isopropylimino)-2,5-cyclohexadien-1-ylidene]aniline (52870-43-6,73334-92-6) + ethyl 2-sulfanylacetate (623-51-8) → ethyl 2-{[5-anilino-2-(isopropylamino)phenyl]sulfanyl}acetate (371965-85-4)

Guidance literature:

With air; In ethanol; for 20h;

DOI:10.1021/jo0101959

Reference yield:

N-phenyl-N'-isopropyl-p-phenylenediamine (101-72-4) → ethyl 2-{[5-anilino-2-(isopropylamino)phenyl]sulfanyl}acetate (371965-85-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 99 percent / Ag₂O; MgSO₄ / toluene / 20 h

2: 94 percent / air / ethanol / 20 h

With air; magnesium sulfate; silver(l) oxide; In ethanol; toluene;

DOI:10.1021/jo0101959

Reference yield: 89.0%

ethyl 2-{[5-anilino-2-(isopropylamino)phenyl]sulfanyl}acetate (371965-85-4) → 7-anilino-4-isopropyl-2H-1,4-benzothiazin-3(4H)-one

Guidance literature:

With trifluoroacetic acid; at 70 ℃; for 20h;

DOI:10.1021/jo0101959

upstream raw materials:

N-[4-(isopropylimino)-2,5-cyclohexadien-1-ylidene]aniline

ethyl 2-sulfanylacetate

N-phenyl-N'-isopropyl-p-phenylenediamine