tricyclo[3.3.1.1^3,7]decane-2-spiro-2'-(4',4'-diphenyl-1',3'-oxathiolan-5'-one)

Base Information

Chemical Name:tricyclo[3.3.1.1^3,7]decane-2-spiro-2'-(4',4'-diphenyl-1',3'-oxathiolan-5'-one)
CAS No.:207285-51-6
Molecular Formula:C₂₄H₂₄O₂S
Molecular Weight:376.519
Hs Code.:

tricyclo[3.3.1.1<sup>3,7</sup>]decane-2-spiro-2'-(4',4'-diphenyl-1',3'-oxathiolan-5'-one)

Synonyms:tricyclo[3.3.1.1^3,7]decane-2-spiro-2'-(4',4'-diphenyl-1',3'-oxathiolan-5'-one)

Suppliers and Price of tricyclo[3.3.1.1^3,7]decane-2-spiro-2'-(4',4'-diphenyl-1',3'-oxathiolan-5'-one)

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Chemical Property of tricyclo[3.3.1.1^3,7]decane-2-spiro-2'-(4',4'-diphenyl-1',3'-oxathiolan-5'-one)

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Technology Process of tricyclo[3.3.1.1^3,7]decane-2-spiro-2'-(4',4'-diphenyl-1',3'-oxathiolan-5'-one)

There total 3 articles about tricyclo[3.3.1.1^3,7]decane-2-spiro-2'-(4',4'-diphenyl-1',3'-oxathiolan-5'-one) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 700-58-3
2-Adamantanone

: 4695-15-2
2,2-diphenyl-2-mercaptoacetic acid

: 207285-51-6
tricyclo[3.3.1.1^3,7]decane-2-spiro-2'-(4',4'-diphenyl-1',3'-oxathiolan-5'-one)

Guidance literature:: With toluene-4-sulfonic acid; In benzene; for 8h; Heating;
DOI:10.1139/v97-201

Reference yield:

: 95702-21-9
diphenyl-phenylcarbamoylsulfanyl-acetic acid

: 207285-51-6
tricyclo[3.3.1.1^3,7]decane-2-spiro-2'-(4',4'-diphenyl-1',3'-oxathiolan-5'-one)

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / 10percent aq. KOH / 5 h / Heating

2: 84 percent / p-TsOH / benzene / 8 h / Heating

With potassium hydroxide; toluene-4-sulfonic acid; In benzene;
DOI:10.1139/v97-201

Reference yield:

: 76-93-7
Benzilic acid

: 207285-51-6
tricyclo[3.3.1.1^3,7]decane-2-spiro-2'-(4',4'-diphenyl-1',3'-oxathiolan-5'-one)

Guidance literature:: Multi-step reaction with 3 steps

1: 62 percent / H₂SO₄ / acetic acid / 4 h / 0 - 20 °C

2: 87 percent / 10percent aq. KOH / 5 h / Heating

3: 84 percent / p-TsOH / benzene / 8 h / Heating

With potassium hydroxide; sulfuric acid; toluene-4-sulfonic acid; In acetic acid; benzene;
DOI:10.1139/v97-201