C₃₄H₃₃IO₇

Base Information

Chemical Name:C₃₄H₃₃IO₇
CAS No.:1193357-61-7
Molecular Formula:C₃₄H₃₃IO₇
Molecular Weight:680.536
Hs Code.:

C<sub>34</sub>H<sub>33</sub>IO<sub>7</sub>

Synonyms:C₃₄H₃₃IO₇

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₄H₃₃IO₇

Chemical Property:

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Technology Process of C₃₄H₃₃IO₇

There total 12 articles about C₃₄H₃₃IO₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 3,5-bis-benzyloxy-2-iodo-phenol

: 1239861-07-4
C₁₄H₁₈O₅

: 1193357-61-7
C₃₄H₃₃IO₇

Guidance literature:: With tributylphosphine; diamide; In toluene; at 0 - 20 ℃; for 2.5h; stereospecific reaction; Inert atmosphere;
DOI:10.1246/cl.2009.934

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1193357-61-7
C₃₄H₃₃IO₇

Guidance literature:: Multi-step reaction with 3 steps

1.1: dmap / dichloromethane / 1 h / 20 °C / Inert atmosphere

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

2.2: Inert atmosphere

3.1: tributylphosphine; diamide / toluene / 2.5 h / 0 - 20 °C / Inert atmosphere

With dmap; tributylphosphine; diamide; tetrabutyl ammonium fluoride; In tetrahydrofuran; dichloromethane; toluene; 3.1: |Mitsunobu Displacement;
DOI:10.1246/cl.2009.934

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 1193357-61-7
C₃₄H₃₃IO₇

Guidance literature:: Multi-step reaction with 11 steps

1.1: potassium carbonate / acetone / 2 h / Reflux; Inert atmosphere

2.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 °C / Inert atmosphere

2.2: 16 h / 0 °C / Inert atmosphere

3.1: diisobutylaluminium hydride / tetrahydrofuran / 2 h / -78 °C / Inert atmosphere

3.2: 0 - 20 °C / Inert atmosphere

4.1: methanesulfonamide; AD-mix β / water; tert-butyl alcohol / 3.8 h / 0 °C / Inert atmosphere

5.1: pyridine / dichloromethane / 29 h / 0 - 20 °C / Inert atmosphere

6.1: potassium carbonate / methanol / 3 h / 0 °C / Inert atmosphere

7.1: 1H-imidazole / N,N-dimethyl-formamide / 2 h / 0 - 20 °C / Inert atmosphere

8.1: 10 wt% Pd(OH)2 on carbon; hydrogen / ethyl acetate / 6.5 h / 20 °C

9.1: dmap / dichloromethane / 1 h / 20 °C / Inert atmosphere

10.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

10.2: Inert atmosphere

11.1: tributylphosphine; diamide / toluene / 2.5 h / 0 - 20 °C / Inert atmosphere

With pyridine; 1H-imidazole; dmap; tributylphosphine; methanesulfonamide; diamide; AD-mix β; 10 wt% Pd(OH)2 on carbon; tetrabutyl ammonium fluoride; hydrogen; sodium hydride; diisobutylaluminium hydride; potassium carbonate; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetone; toluene; mineral oil; tert-butyl alcohol; 11.1: |Mitsunobu Displacement;
DOI:10.1246/cl.2009.934