22β-(4-(4-morpholylmethyl)benzyloxy)-3β,24-isopropylidenedioxyolean-12-ene

Base Information

Chemical Name:22β-(4-(4-morpholylmethyl)benzyloxy)-3β,24-isopropylidenedioxyolean-12-ene
CAS No.:1312328-85-0
Molecular Formula:C₄₅H₆₉NO₄
Molecular Weight:688.047
Hs Code.:

Synonyms:22β-(4-(4-morpholylmethyl)benzyloxy)-3β,24-isopropylidenedioxyolean-12-ene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 22β-(4-(4-morpholylmethyl)benzyloxy)-3β,24-isopropylidenedioxyolean-12-ene

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Technology Process of 22β-(4-(4-morpholylmethyl)benzyloxy)-3β,24-isopropylidenedioxyolean-12-ene

There total 4 articles about 22β-(4-(4-morpholylmethyl)benzyloxy)-3β,24-isopropylidenedioxyolean-12-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 110-91-8,99108-56-2
morpholine

: 1312328-59-8
22β-(4-formylbenzyloxy)-3β,24-isopropylidenedioxyolean-12-ene

: 1312328-85-0
22β-(4-(4-morpholylmethyl)benzyloxy)-3β,24-isopropylidenedioxyolean-12-ene

Guidance literature:: morpholine; 22β-(4-formylbenzyloxy)-3β,24-isopropylidenedioxyolean-12-ene; With magnesium sulfate; acetic acid; In 1,2-dichloro-ethane; at 20 ℃; for 0.166667h;

With sodium tris(acetoxy)borohydride; acetic acid; In 1,2-dichloro-ethane; at 20 ℃; Cooling with ice;

With sodium hydrogencarbonate; In water; 1,2-dichloro-ethane;

Reference yield:

: 1311130-41-2
22β-(4-iodobenzyloxy)-3β,24-isopropylidenedioxyolean-12-ene

: 1312328-85-0
22β-(4-(4-morpholylmethyl)benzyloxy)-3β,24-isopropylidenedioxyolean-12-ene

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / hexane; tetrahydrofuran / 0.08 h / -78 °C

1.2: 0.58 h / -78 - -40 °C

2.1: magnesium sulfate; acetic acid / 1,2-dichloro-ethane / 0.17 h / 20 °C

2.2: 20 °C / Cooling with ice

With n-butyllithium; magnesium sulfate; acetic acid; In tetrahydrofuran; hexane; 1,2-dichloro-ethane;

Reference yield:

: 104235-58-7
22β-hydroxy-3β,24-isopropylidenedioxyolean-12-ene

: 1312328-85-0
22β-(4-(4-morpholylmethyl)benzyloxy)-3β,24-isopropylidenedioxyolean-12-ene

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.25 h / 20 °C

1.2: 1.17 h / 70 °C

2.1: n-butyllithium / hexane; tetrahydrofuran / 0.08 h / -78 °C

2.2: 0.58 h / -78 - -40 °C

3.1: magnesium sulfate; acetic acid / 1,2-dichloro-ethane / 0.17 h / 20 °C

3.2: 20 °C / Cooling with ice

With n-butyllithium; sodium hydride; magnesium sulfate; acetic acid; In tetrahydrofuran; hexane; 1,2-dichloro-ethane; N,N-dimethyl-formamide; mineral oil;