Technology Process of C19H28BrN3O3
There total 5 articles about C19H28BrN3O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
palladium on activated charcoal; hydrogen;
In
methanol;
at 20 ℃;
under 15201 Torr;
Inert atmosphere;
Sealed tube;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: triethylamine; HATU / dichloromethane / 0.25 h / 20 °C
1.2: 1 h / 20 °C
2.1: hydrogen / platinum on activated charcoal / methanol / 1034.32 Torr
With
hydrogen; triethylamine; HATU;
platinum on activated charcoal;
In
methanol; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium hydroxide; water / tetrahydrofuran; methanol / 5 h / 80 °C
1.2: pH 2
2.1: triethylamine / dichloromethane / 0.25 h / 20 °C / Inert atmosphere
2.2: 3 h / 20 °C
3.1: triethylamine; HATU / dichloromethane / 0.25 h / 20 °C
3.2: 1 h / 20 °C
4.1: hydrogen / platinum on activated charcoal / methanol / 1034.32 Torr
With
water; hydrogen; triethylamine; HATU; potassium hydroxide;
platinum on activated charcoal;
In
tetrahydrofuran; methanol; dichloromethane;