N¹-phthalamic acid-N⁴-(4-benzyloxycarbonyl-1-benzoic acid)-N⁸-Boc-spermidine

Base Information

Chemical Name:N¹-phthalamic acid-N⁴-(4-benzyloxycarbonyl-1-benzoic acid)-N⁸-Boc-spermidine
CAS No.:201211-60-1
Molecular Formula:C₂₉H₃₇N₃O₉
Molecular Weight:571.627
Hs Code.:

N<sup>1</sup>-phthalamic acid-N<sup>4</sup>-(4-benzyloxycarbonyl-1-benzoic acid)-N<sup>8</sup>-Boc-spermidine

Synonyms:N¹-phthalamic acid-N⁴-(4-benzyloxycarbonyl-1-benzoic acid)-N⁸-Boc-spermidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N¹-phthalamic acid-N⁴-(4-benzyloxycarbonyl-1-benzoic acid)-N⁸-Boc-spermidine

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Technology Process of N¹-phthalamic acid-N⁴-(4-benzyloxycarbonyl-1-benzoic acid)-N⁸-Boc-spermidine

There total 1 articles about N¹-phthalamic acid-N⁴-(4-benzyloxycarbonyl-1-benzoic acid)-N⁸-Boc-spermidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 191277-08-4
4-({(4-tert-Butoxycarbonylamino-butyl)-[3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-propyl]-carbamoyloxy}-methyl)-benzoic acid methyl ester

: 201211-60-1
N¹-phthalamic acid-N⁴-(4-benzyloxycarbonyl-1-benzoic acid)-N⁸-Boc-spermidine

Guidance literature:: With sodium hydroxide; In 1,4-dioxane; for 1.5h; Ambient temperature;
DOI:10.1016/S0040-4020(97)10156-9

Reference yield:

: 201211-60-1
N¹-phthalamic acid-N⁴-(4-benzyloxycarbonyl-1-benzoic acid)-N⁸-Boc-spermidine

: 4-{[(3-Amino-propyl)-(4-tert-butoxycarbonylamino-butyl)-carbamoyloxy]-methyl}-benzoic acid

Guidance literature:: With hydrazine hydrate; In ethanol; at 80 ℃; for 21h;
DOI:10.1016/S0040-4020(97)10156-9

Reference yield:

: 201211-60-1
N¹-phthalamic acid-N⁴-(4-benzyloxycarbonyl-1-benzoic acid)-N⁸-Boc-spermidine

: 191277-10-8
4-({(4-tert-Butoxycarbonylamino-butyl)-[3-(9H-fluoren-9-ylmethoxycarbonylamino)-propyl]-carbamoyloxy}-methyl)-benzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: N₂H₄*H₂O / ethanol / 21 h / 80 °C

2: NaHCO₃ / dioxane

With sodium hydrogencarbonate; hydrazine hydrate; In 1,4-dioxane; ethanol;
DOI:10.1016/S0040-4020(97)10156-9