C₄₃H₅₃NO₁₀

Base Information

Chemical Name:C₄₃H₅₃NO₁₀
CAS No.:1265221-66-6
Molecular Formula:C₄₃H₅₃NO₁₀
Molecular Weight:743.895
Hs Code.:

C<sub>43</sub>H<sub>53</sub>NO<sub>10</sub>

Synonyms:C₄₃H₅₃NO₁₀

Suppliers and Price of C₄₃H₅₃NO₁₀

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₄₃H₅₃NO₁₀

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₄₃H₅₃NO₁₀

There total 18 articles about C₄₃H₅₃NO₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1265221-65-5
C₁₂H₁₉BO₄

: 1265221-64-4
C₃₁H₃₆BrNO₈

: 1265221-66-6
C₄₃H₅₃NO₁₀

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutylammomium bromide; potassium carbonate; In tetrahydrofuran; water; at 90 ℃; for 1.5h; Inert atmosphere; Microwave irradiation;
DOI:10.1002/ejoc.201001133

Reference yield:

: 1265221-55-3
C₈H₈INO₄

: 1265221-66-6
C₄₃H₅₃NO₁₀

Guidance literature:: Multi-step reaction with 4 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutylammomium bromide; potassium carbonate / tetrahydrofuran; water / 1 h / 60 °C / Inert atmosphere; Microwave irradiation

2: N-Bromosuccinimide / N,N-dimethyl-formamide / 14 h / 18 °C

3: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 1 h / 18 °C

4: tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutylammomium bromide; potassium carbonate / tetrahydrofuran; water / 1.5 h / 90 °C / Inert atmosphere; Microwave irradiation

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; di-isopropyl azodicarboxylate; tetrabutylammomium bromide; potassium carbonate; triphenylphosphine; In tetrahydrofuran; water; N,N-dimethyl-formamide; 3: Mitsunobu reaction / 4: Suzuki coupling;
DOI:10.1002/ejoc.201001133

Reference yield:

: 1265221-59-7
2-(3,4-diisopropoxyphenoxy)tetrahydro-2H-pyran

: 1265221-66-6
C₄₃H₅₃NO₁₀

Guidance literature:: Multi-step reaction with 7 steps

1.1: N-Bromosuccinimide; sodium carbonate / N,N-dimethyl-formamide / 3 h / 0 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 12.66 h / -78 - 18 °C / Inert atmosphere

3.1: hydrogenchloride; water / tetrahydrofuran; hexane / 0.25 h

3.2: 24 h

4.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutylammomium bromide; potassium carbonate / tetrahydrofuran; water / 1 h / 60 °C / Inert atmosphere; Microwave irradiation

5.1: N-Bromosuccinimide / N,N-dimethyl-formamide / 14 h / 18 °C

6.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 1 h / 18 °C

7.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutylammomium bromide; potassium carbonate / tetrahydrofuran; water / 1.5 h / 90 °C / Inert atmosphere; Microwave irradiation

With hydrogenchloride; N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; di-isopropyl azodicarboxylate; tetrabutylammomium bromide; water; sodium carbonate; potassium carbonate; triphenylphosphine; In tetrahydrofuran; hexane; water; N,N-dimethyl-formamide; 6.1: Mitsunobu reaction / 7.1: Suzuki coupling;
DOI:10.1002/ejoc.201001133