6-phenyl-2,3,4,4a,5,6-hexahydro-1H,11H-4,5-ethanopyrimido<1,2-a>quinazoline

Base Information

Chemical Name:6-phenyl-2,3,4,4a,5,6-hexahydro-1H,11H-4,5-ethanopyrimido<1,2-a>quinazoline
CAS No.:76896-31-6
Molecular Formula:C₁₉H₂₁N₃
Molecular Weight:291.396
Hs Code.:

Synonyms:6-phenyl-2,3,4,4a,5,6-hexahydro-1H,11H-4,5-ethanopyrimido<1,2-a>quinazoline

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Chemical Property of 6-phenyl-2,3,4,4a,5,6-hexahydro-1H,11H-4,5-ethanopyrimido<1,2-a>quinazoline

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Technology Process of 6-phenyl-2,3,4,4a,5,6-hexahydro-1H,11H-4,5-ethanopyrimido<1,2-a>quinazoline

There total 4 articles about 6-phenyl-2,3,4,4a,5,6-hexahydro-1H,11H-4,5-ethanopyrimido<1,2-a>quinazoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 76896-25-8
6-Phenyl-2,3,4,5-tetrahydro-1H,6H-5a,10b-diaza-3a-azonia-acephenanthrylene; chloride

: 76896-31-6
6-phenyl-2,3,4,4a,5,6-hexahydro-1H,11H-4,5-ethanopyrimido<1,2-a>quinazoline

Guidance literature:: With sodium tetrahydroborate; In ethanol; for 1h; Ambient temperature;
DOI:10.1248/cpb.28.2587

Reference yield:

: 76896-23-6
1-(3-chloropropyl)-5-phenyl-1,2,3,5-tetrahydroimidazo<2,1-b>quinazoline

: 76896-31-6
6-phenyl-2,3,4,4a,5,6-hexahydro-1H,11H-4,5-ethanopyrimido<1,2-a>quinazoline

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / ethanol / 3 h / Heating

2: 93 percent / NaBH₄ / aq. ethanol / 1 h / Ambient temperature

With sodium tetrahydroborate; In ethanol;
DOI:10.1248/cpb.28.2587

Reference yield:

: 76896-20-3
1-(3-hydroxypropyl)-5-phenyl-1,2,3,5-tetrahydroimidazol<2,1-b>quinazoline

: 76896-31-6
6-phenyl-2,3,4,4a,5,6-hexahydro-1H,11H-4,5-ethanopyrimido<1,2-a>quinazoline

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / thionyl chloride / CHCl₃ / 2 h / Ambient temperature

2: 93 percent / ethanol / 3 h / Heating

3: 93 percent / NaBH₄ / aq. ethanol / 1 h / Ambient temperature

With sodium tetrahydroborate; thionyl chloride; In ethanol; chloroform;
DOI:10.1248/cpb.28.2587