Technology Process of C42H62N2O11Si2
There total 4 articles about C42H62N2O11Si2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium diethoxyaluminum hydride;
In
diethyl ether;
at -78 ℃;
for 0.25h;
DOI:10.1021/ol0056729
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 2-chloro-1,3-dimethylimidazolidinium hexafluorophosphate; 1-hydroxy-7-azabenzotriazole; triethylamine / tetrahydrofuran; CH2Cl2 / 24 h / 0 - 23 °C
2: Cs2CO3 / dimethylformamide / 2 h / 23 °C
3: 95 percent / lithium diethoxyaluminium hydride / diethyl ether / 0.25 h / -78 °C
With
1-hydroxy-7-aza-benzotriazole; 2-chloro-1,3-dimethylimidazolidinium hexafluorophosphate; caesium carbonate; lithium diethoxyaluminum hydride; triethylamine;
In
tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
1: Acylation / 2: Etherification / 3: Reduction;
DOI:10.1021/ol0056729
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 2-chloro-1,3-dimethylimidazolidinium hexafluorophosphate; 1-hydroxy-7-azabenzotriazole; triethylamine / tetrahydrofuran; CH2Cl2 / 24 h / 0 - 23 °C
2: Cs2CO3 / dimethylformamide / 2 h / 23 °C
3: 95 percent / lithium diethoxyaluminium hydride / diethyl ether / 0.25 h / -78 °C
With
1-hydroxy-7-aza-benzotriazole; 2-chloro-1,3-dimethylimidazolidinium hexafluorophosphate; caesium carbonate; lithium diethoxyaluminum hydride; triethylamine;
In
tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
1: Acylation / 2: Etherification / 3: Reduction;
DOI:10.1021/ol0056729
