C₃₈H₅₂O₇Si

Base Information

Chemical Name:C₃₈H₅₂O₇Si
CAS No.:1286242-13-4
Molecular Formula:C₃₈H₅₂O₇Si
Molecular Weight:648.912
Hs Code.:

C<sub>38</sub>H<sub>52</sub>O<sub>7</sub>Si

Synonyms:C₃₈H₅₂O₇Si

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Chemical Property of C₃₈H₅₂O₇Si

Chemical Property:

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Technology Process of C₃₈H₅₂O₇Si

There total 17 articles about C₃₈H₅₂O₇Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1286242-12-3
C₃₆H₄₈O₆Si

: 107-30-2
chloromethyl methyl ether

: 1286242-13-4
C₃₈H₅₂O₇Si

Guidance literature:: With N-ethyl-N,N-diisopropylamine; sodium iodide; In 1,2-dimethoxyethane; Reflux;
DOI:10.3987/COM-10-12106

Reference yield:

: 1286241-97-1
C₃₀H₄₈O₄Si₂

: 1286242-13-4
C₃₈H₅₂O₇Si

Guidance literature:: Multi-step reaction with 11 steps

1: Dess-Martin periodane / dichloromethane

2: 2,3-dicyano-5,6-dichloro-p-benzoquinone / tetrahydrofuran; water

3: trimethylaluminum / dichloromethane; water / -50 °C

4: toluene-4-sulfonic acid / benzene / Reflux

5: diisobutylaluminium hydride / tetrahydrofuran / 0 °C

6: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2R,3R)-tartrate / dichloromethane / -30 °C

7: copper(l) cyanide / diethyl ether / -50 - -30 °C

8: 2,2,6,6-tetramethyl-piperidine-N-oxyl; [bis(acetoxy)iodo]benzene / dichloromethane

9: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / tetrahydrofuran; water; tert-butyl alcohol

10: diethyl ether / 0 °C

11: N-ethyl-N,N-diisopropylamine; sodium iodide / 1,2-dimethoxyethane / Reflux

With titanium(IV) isopropylate; tert.-butylhydroperoxide; 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; diethyl (2R,3R)-tartrate; [bis(acetoxy)iodo]benzene; trimethylaluminum; copper(l) cyanide; diisobutylaluminium hydride; Dess-Martin periodane; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium iodide; In tetrahydrofuran; 1,2-dimethoxyethane; diethyl ether; dichloromethane; water; tert-butyl alcohol; benzene; 1: Dess-Martin oxidation / 1: Wittig reaction / 6: Katsuki-Sharpless epoxidation;
DOI:10.3987/COM-10-12106

Reference yield:

: 1286241-95-9
C₃₀H₄₈O₃Si₂

: 1286242-13-4
C₃₈H₅₂O₇Si

Guidance literature:: Multi-step reaction with 12 steps

1: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2R,3R)-tartrate / dichloromethane / -30 °C

2: Dess-Martin periodane / dichloromethane

3: 2,3-dicyano-5,6-dichloro-p-benzoquinone / tetrahydrofuran; water

4: trimethylaluminum / dichloromethane; water / -50 °C

5: toluene-4-sulfonic acid / benzene / Reflux

6: diisobutylaluminium hydride / tetrahydrofuran / 0 °C

7: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2R,3R)-tartrate / dichloromethane / -30 °C

8: copper(l) cyanide / diethyl ether / -50 - -30 °C

9: 2,2,6,6-tetramethyl-piperidine-N-oxyl; [bis(acetoxy)iodo]benzene / dichloromethane

10: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / tetrahydrofuran; water; tert-butyl alcohol

11: diethyl ether / 0 °C

12: N-ethyl-N,N-diisopropylamine; sodium iodide / 1,2-dimethoxyethane / Reflux

With titanium(IV) isopropylate; tert.-butylhydroperoxide; 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; diethyl (2R,3R)-tartrate; [bis(acetoxy)iodo]benzene; trimethylaluminum; copper(l) cyanide; diisobutylaluminium hydride; Dess-Martin periodane; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium iodide; In tetrahydrofuran; 1,2-dimethoxyethane; diethyl ether; dichloromethane; water; tert-butyl alcohol; benzene; 1: Katsuki-Sharpless epoxidation / 2: Dess-Martin oxidation / 2: Wittig reaction / 7: Katsuki-Sharpless epoxidation;
DOI:10.3987/COM-10-12106