C₁₇H₂₅NO₃S

Base Information

Chemical Name:C₁₇H₂₅NO₃S
CAS No.:1268630-72-3
Molecular Formula:C₁₇H₂₅NO₃S
Molecular Weight:323.456
Hs Code.:

C<sub>17</sub>H<sub>25</sub>NO<sub>3</sub>S

Synonyms:C₁₇H₂₅NO₃S

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Chemical Property of C₁₇H₂₅NO₃S

Chemical Property:

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Technology Process of C₁₇H₂₅NO₃S

There total 6 articles about C₁₇H₂₅NO₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1268630-63-2
C₁₇H₂₇NO₄S

: 1268630-72-3
C₁₇H₂₅NO₃S

Guidance literature:: With 1,1'-bis-(diphenylphosphino)ferrocene; dimethylsulfide gold(I) chloride; silver trifluoromethanesulfonate; In dichloromethane; toluene; at 20 ℃; for 6h; optical yield given as %de; diastereoselective reaction; Darkness;
DOI:10.1002/chem.201002606

Reference yield:

: 316363-73-2
(S)-O-(tert-butyldimethylsilyl)-N-(4-methylbenzenesulfonyl)-leucinol

: 1268630-72-3
C₁₇H₂₅NO₃S

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.25 h / 0 °C / Inert atmosphere

1.2: 16 h / Inert atmosphere; Reflux

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 6 h / 20 °C

3.1: 1,1'-bis-(diphenylphosphino)ferrocene; dimethylsulfide gold(I) chloride; silver trifluoromethanesulfonate / dichloromethane; toluene / 6 h / 20 °C / Darkness

With 1,1'-bis-(diphenylphosphino)ferrocene; dimethylsulfide gold(I) chloride; tetrabutyl ammonium fluoride; silver trifluoromethanesulfonate; sodium hydride; In tetrahydrofuran; dichloromethane; toluene; mineral oil;
DOI:10.1002/chem.201002606

Reference yield:

: 7533-40-6,14438-11-0
(S)-2-amino-4-methylpentan-1-ol

: 1268630-72-3
C₁₇H₂₅NO₃S

Guidance literature:: Multi-step reaction with 5 steps

1.1: triethylamine / dichloromethane / 16 h / 20 °C

2.1: dmap; triethylamine / dichloromethane / 16 h / 0 - 20 °C

3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.25 h / 0 °C / Inert atmosphere

3.2: 16 h / Inert atmosphere; Reflux

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 6 h / 20 °C

5.1: 1,1'-bis-(diphenylphosphino)ferrocene; dimethylsulfide gold(I) chloride; silver trifluoromethanesulfonate / dichloromethane; toluene / 6 h / 20 °C / Darkness

With dmap; 1,1'-bis-(diphenylphosphino)ferrocene; dimethylsulfide gold(I) chloride; tetrabutyl ammonium fluoride; silver trifluoromethanesulfonate; sodium hydride; triethylamine; In tetrahydrofuran; dichloromethane; toluene; mineral oil;
DOI:10.1002/chem.201002606