4-O-<3',4'-O-cyclohexylidene-2'-deoxy-(tosylamino)-α-D-gluco-hexodialdo-1',5'-pyranosyl>-5,6-O-cyclohexylidene-1,3-di-N-tosyl-2-deoxystreptamine

Base Information

Chemical Name:4-O-<3',4'-O-cyclohexylidene-2'-deoxy-(tosylamino)-α-D-gluco-hexodialdo-1',5'-pyranosyl>-5,6-O-cyclohexylidene-1,3-di-N-tosyl-2-deoxystreptamine
CAS No.:88970-29-0
Molecular Formula:C₄₅H₅₇N₃O₁₃S₃
Molecular Weight:944.158
Hs Code.:

Synonyms:4-O-<3',4'-O-cyclohexylidene-2'-deoxy-(tosylamino)-α-D-gluco-hexodialdo-1',5'-pyranosyl>-5,6-O-cyclohexylidene-1,3-di-N-tosyl-2-deoxystreptamine

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Chemical Property of 4-O-<3',4'-O-cyclohexylidene-2'-deoxy-(tosylamino)-α-D-gluco-hexodialdo-1',5'-pyranosyl>-5,6-O-cyclohexylidene-1,3-di-N-tosyl-2-deoxystreptamine

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Technology Process of 4-O-<3',4'-O-cyclohexylidene-2'-deoxy-(tosylamino)-α-D-gluco-hexodialdo-1',5'-pyranosyl>-5,6-O-cyclohexylidene-1,3-di-N-tosyl-2-deoxystreptamine

There total 2 articles about 4-O-<3',4'-O-cyclohexylidene-2'-deoxy-(tosylamino)-α-D-gluco-hexodialdo-1',5'-pyranosyl>-5,6-O-cyclohexylidene-1,3-di-N-tosyl-2-deoxystreptamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 88970-28-9
3',4':5,6-di-O-cyclohexylidene-6',6'-di-N-methyl-1,2',3-tri-N-tosylneamine 6'-N-oxide

: 88970-29-0
4-O-<3',4'-O-cyclohexylidene-2'-deoxy-(tosylamino)-α-D-gluco-hexodialdo-1',5'-pyranosyl>-5,6-O-cyclohexylidene-1,3-di-N-tosyl-2-deoxystreptamine

Guidance literature:: With benzoyl chloride; N-ethyl-N,N-diisopropylamine; In acetone; 1) RT, 3 min.; 2) 40 deg C, 10 min.;
DOI:10.1246/bcsj.57.529

Reference yield:

: 91613-41-1
C₄₇H₆₄N₄O₁₂S₃

: 88970-29-0
4-O-<3',4'-O-cyclohexylidene-2'-deoxy-(tosylamino)-α-D-gluco-hexodialdo-1',5'-pyranosyl>-5,6-O-cyclohexylidene-1,3-di-N-tosyl-2-deoxystreptamine

Guidance literature:: Multi-step reaction with 2 steps

1: 47.1 percent / m-chloroperbenzoic acid / CHCl₃ / 1 h / Ambient temperature

2: 75 percent / N,N-diisopropylethylamine, benzoyl chloride / acetone / 1) RT, 3 min.; 2) 40 deg C, 10 min.

With benzoyl chloride; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; In chloroform; acetone;
DOI:10.1246/bcsj.57.529