C₁₁H₁₃BrFNO₄

Base Information

• Chemical Name: C₁₁H₁₃BrFNO₄
• CAS No.: 1374109-85-9
• Molecular Formula: C₁₁H₁₃BrFNO₄
• Molecular Weight: 322.131
• Mol file: 1374109-85-9.mol

Synonyms:C₁₁H₁₃BrFNO₄

Chemical Property of C₁₁H₁₃BrFNO₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₁H₁₃BrFNO₄

There total 4 articles about C₁₁H₁₃BrFNO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

C11H12BrNO4 (1374109-84-8) → C11H13BrFNO4 (1374109-85-9)

Guidance literature:

With potassium hydrogen bifluoride; tetra-n-butylammonium dihydrogen trifluoride; at 120 ℃; for 6h;

Reference yield:

4-bromo-2-fluoronitrobenzene (321-23-3) → C11H13BrFNO4 (1374109-85-9)

Guidance literature:

Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 20 °C / Reflux; Inert atmosphere

1.2: 16 h / 20 °C

2.1: 3-chloro-benzenecarboperoxoic acid / chloroform / 48 h / 20 °C

3.1: tetra-n-butylammonium dihydrogen trifluoride; potassium hydrogen bifluoride / 6 h / 120 °C

With potassium hydrogen bifluoride; sodium hydride; tetra-n-butylammonium dihydrogen trifluoride; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; chloroform; mineral oil;

Reference yield:

2-methyl-3-buten-2-ol (115-18-4) → C11H13BrFNO4 (1374109-85-9)

Guidance literature:

Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 20 °C / Reflux; Inert atmosphere

1.2: 16 h / 20 °C

2.1: 3-chloro-benzenecarboperoxoic acid / chloroform / 48 h / 20 °C

3.1: tetra-n-butylammonium dihydrogen trifluoride; potassium hydrogen bifluoride / 6 h / 120 °C

With potassium hydrogen bifluoride; sodium hydride; tetra-n-butylammonium dihydrogen trifluoride; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; chloroform; mineral oil;

upstream raw materials:

4-bromo-2-fluoronitrobenzene

2-methyl-3-buten-2-ol

C₁₁H₁₂BrNO₃

C₁₁H₁₂BrNO₄

Downstream raw materials:

C₁₇H₂₅BFNO₆

C₂₀H₁₈FN₃O₆