14-[4-(2-{2-[2-(4-tritylphenoxy)ethoxy]ethoxy}ethoxy)phenoxy]-6,9,12-trioxatetradecan-2-one ethylene acetal

Base Information

Chemical Name:14-[4-(2-{2-[2-(4-tritylphenoxy)ethoxy]ethoxy}ethoxy)phenoxy]-6,9,12-trioxatetradecan-2-one ethylene acetal
CAS No.:145839-37-8
Molecular Formula:C₅₀H₆₀O₁₀
Molecular Weight:821.02
Hs Code.:

Synonyms:14-[4-(2-{2-[2-(4-tritylphenoxy)ethoxy]ethoxy}ethoxy)phenoxy]-6,9,12-trioxatetradecan-2-one ethylene acetal

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Chemical Property of 14-[4-(2-{2-[2-(4-tritylphenoxy)ethoxy]ethoxy}ethoxy)phenoxy]-6,9,12-trioxatetradecan-2-one ethylene acetal

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Technology Process of 14-[4-(2-{2-[2-(4-tritylphenoxy)ethoxy]ethoxy}ethoxy)phenoxy]-6,9,12-trioxatetradecan-2-one ethylene acetal

There total 6 articles about 14-[4-(2-{2-[2-(4-tritylphenoxy)ethoxy]ethoxy}ethoxy)phenoxy]-6,9,12-trioxatetradecan-2-one ethylene acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 5978-08-5
1-chloro-4-(1,3-dioxolane)-n-pentane

: 145839-41-4
2-<2-<2-<4-<2-<2-<2-(4-triphenylmethylphenoxy)ethoxy>ethoxy>ethoxy>phenoxy>ethoxy>ethoxy>ethanol

: 145839-37-8
14-[4-(2-{2-[2-(4-tritylphenoxy)ethoxy]ethoxy}ethoxy)phenoxy]-6,9,12-trioxatetradecan-2-one ethylene acetal

Guidance literature:: With sodium hydride; In tetrahydrofuran; Heating;
DOI:10.1002/chem.19970030719

Reference yield:

: 978-86-9
4-tritylphenol

: 145839-37-8
14-[4-(2-{2-[2-(4-tritylphenoxy)ethoxy]ethoxy}ethoxy)phenoxy]-6,9,12-trioxatetradecan-2-one ethylene acetal

Guidance literature:: Multi-step reaction with 3 steps

1: K₂CO₃ / dimethylformamide / 96 h / 70 °C

2: TBAF / tetrahydrofuran / 3 h / 70 °C

3: 51 percent / NaH / tetrahydrofuran / Heating

With tetrabutyl ammonium fluoride; sodium hydride; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1002/chem.19970030719

Reference yield:

: 134881-72-4
1,4-bis-(2-(2-(2-hydroxyethoxy)ethoxy)ethoxy)benzene

: 145839-37-8
14-[4-(2-{2-[2-(4-tritylphenoxy)ethoxy]ethoxy}ethoxy)phenoxy]-6,9,12-trioxatetradecan-2-one ethylene acetal

Guidance literature:: Multi-step reaction with 5 steps

1: 38 percent / imidazole / dimethylformamide / 3 h / Ambient temperature

2: 84 percent / Et₃N, DMAP / CH₂Cl₂ / 15 h / 4 °C

3: K₂CO₃ / dimethylformamide / 96 h / 70 °C

4: TBAF / tetrahydrofuran / 3 h / 70 °C

5: 51 percent / NaH / tetrahydrofuran / Heating

With 1H-imidazole; dmap; tetrabutyl ammonium fluoride; sodium hydride; potassium carbonate; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.19970030719