4--2(S)-pyrrilidin-2-ylmethoxy>nitrobenzene

Base Information

Chemical Name:4--2(S)-pyrrilidin-2-ylmethoxy>nitrobenzene
CAS No.:199109-26-7
Molecular Formula:C₃₂H₃₈N₂O₅
Molecular Weight:530.664
Hs Code.:

4-<N-<(3R/S)-benzyloxy-2,2,4,6,7-pentamethyl-1-benzofuran-3-ylmethyl>-2(S)-pyrrilidin-2-ylmethoxy>nitrobenzene

Synonyms:4--2(S)-pyrrilidin-2-ylmethoxy>nitrobenzene

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Chemical Property of 4--2(S)-pyrrilidin-2-ylmethoxy>nitrobenzene

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Technology Process of 4--2(S)-pyrrilidin-2-ylmethoxy>nitrobenzene

There total 3 articles about 4--2(S)-pyrrilidin-2-ylmethoxy>nitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 183142-41-8
5-benzyloxy-2,2,4,6,7-pentamethyl-1-benzofuran-3-carbinol

: 199109-26-7
4--2(S)-pyrrilidin-2-ylmethoxy>nitrobenzene

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / Et₃N / CH₂Cl₂ / 3 h / 25 °C

2: 73 percent / 12 h / 120 °C

3: 1.) NaH / 1.) DMF, 25 deg C, 1 h, 2.) DMF, 25 deg C, 3 h

With sodium hydride; triethylamine; In dichloromethane;
DOI:10.1021/jm980549x

Reference yield:

: 187341-65-7
5-benzyloxy-2,2,4,6,7-pentamethyl-1-benzofuran-3-ylmethyl methanesulfonate

: 199109-26-7
4--2(S)-pyrrilidin-2-ylmethoxy>nitrobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / 12 h / 120 °C

2: 1.) NaH / 1.) DMF, 25 deg C, 1 h, 2.) DMF, 25 deg C, 3 h

With sodium hydride;
DOI:10.1021/jm980549x

Reference yield:

: 350-46-9,178603-76-4
4-Fluoronitrobenzene

: 199108-77-5
N-<(3R/S)-5-benzyloxy-2,3-dihydro-2,2,4,6,7-pentamethyl-1-benzofuran-3-ylmethyl>-(2S)-pyrrolidine-2-methanol

: 199109-26-7
4--2(S)-pyrrilidin-2-ylmethoxy>nitrobenzene

Guidance literature:: With sodium hydride; Yield given; Multistep reaction; 1.) DMF, 25 deg C, 1 h, 2.) DMF, 25 deg C, 3 h;
DOI:10.1021/jm980549x