IrC₅(CH₃)5(P(CH₃)3)I(C₆F₅)

Base Information

Chemical Name:IrC₅(CH₃)5(P(CH₃)3)I(C₆F₅)
CAS No.:358720-75-9
Molecular Formula:C₁₉H₂₄F₅IIrP
Molecular Weight:697.49
Hs Code.:

IrC<sub>5</sub>(CH<sub>3</sub>)5(P(CH<sub>3</sub>)3)I(C<sub>6</sub>F<sub>5</sub>)

Synonyms:IrC₅(CH₃)5(P(CH₃)3)I(C₆F₅)

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Chemical Property of IrC₅(CH₃)5(P(CH₃)3)I(C₆F₅)

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Technology Process of IrC₅(CH₃)5(P(CH₃)3)I(C₆F₅)

There total 1 articles about IrC₅(CH₃)5(P(CH₃)3)I(C₆F₅) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 358720-74-8
IrC₅(CH₃)5(CO)I(C₆F₅)

: 594-09-2
trimethylphosphane

: 358720-75-9
IrC₅(CH₃)5(P(CH₃)3)I(C₆F₅)

Guidance literature:: In toluene; (N2); addn. of phosphine to a soln. of iridium complex in toluene, refluxing for 3.5 h, cooling to room temp.; filtration through Celite, evapn., recrystn. (CH2Cl2/hexane); elem. anal.;
DOI:10.1021/om0204787

Reference yield:

: 358720-75-9
IrC₅(CH₃)5(P(CH₃)3)I(C₆F₅)

: 7732-18-5
water

: 358720-76-0
IrC₅(CH₃)5(P(CH₃)3)(H₂O)(C₆F₅)⁽¹⁺⁾

Guidance literature:: With silver trifluoromethanesulfonate; In toluene; Ag)Tf in moist toluene; Hughes, R. P.; Smith, J. M. J. Am. Chem. Soc. 1999, 121, 6084-6085;
DOI:10.1021/ja010992o

Reference yield:

: 16940-66-2
sodium tetrahydroborate

: 358720-75-9
IrC₅(CH₃)5(P(CH₃)3)I(C₆F₅)

: 226882-89-9
(η(5)-C5Me5)(PMe3)Ir(C6F5)(H)

Guidance literature:: In isopropyl alcohol; (N2); refluxing a soln. of iridium complex with hydride in 2-propanol for 4 h; evapn., extn. with hexanes, filtration, evapn.; contaminated with 2-propanol;
DOI:10.1021/om0204787