C₁₄H₁₃ClN₂O

Base Information

Chemical Name:C₁₄H₁₃ClN₂O
CAS No.:1446516-57-9
Molecular Formula:C₁₄H₁₃ClN₂O
Molecular Weight:260.723
Hs Code.:

C<sub>14</sub>H<sub>13</sub>ClN<sub>2</sub>O

Synonyms:C₁₄H₁₃ClN₂O

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Chemical Property of C₁₄H₁₃ClN₂O

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Technology Process of C₁₄H₁₃ClN₂O

There total 6 articles about C₁₄H₁₃ClN₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1449223-56-6
C₁₄H₁₅ClN₂O₂

: 1446516-57-9
C₁₄H₁₃ClN₂O

Guidance literature:: C₁₄H₁₅ClN₂O₂; With hydrogenchloride; acetic acid; In water; at 20 ℃; for 24h;

With sodium hydrogencarbonate; In water; for 0.05h; Reflux;
DOI:10.1016/j.tetlet.2013.05.066

Reference yield:

: 620-02-0
5-Methylfurfural

: 1446516-57-9
C₁₄H₁₃ClN₂O

Guidance literature:: Multi-step reaction with 5 steps

1.1: benzene / 2 h / Reflux; Dean-Stark

2.1: ethanol; sodium tetrahydroborate / 20 °C

3.1: benzene / 1 h / 20 °C

4.1: hydrazine hydrate / ethanol / 0.08 h / Reflux

5.1: hydrogenchloride; acetic acid / water / 24 h / 20 °C

5.2: 0.05 h / Reflux

With hydrogenchloride; sodium tetrahydroborate; ethanol; hydrazine hydrate; acetic acid; In ethanol; water; benzene; 5.2: |Paal-Knorr Pyrrole Synthesis;
DOI:10.1016/j.tetlet.2013.05.066

Reference yield:

: 1446516-45-5
C₂₂H₁₇ClN₂O₄

: 1446516-57-9
C₁₄H₁₃ClN₂O

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrazine hydrate / ethanol / 0.08 h / Reflux

2.1: hydrogenchloride; acetic acid / water / 24 h / 20 °C

2.2: 0.05 h / Reflux

With hydrogenchloride; hydrazine hydrate; acetic acid; In ethanol; water; 2.2: |Paal-Knorr Pyrrole Synthesis;
DOI:10.1016/j.tetlet.2013.05.066