2-(3-dimethylaminocarbonylphenoxy)-6-(2-benzyloxy-5-cyanophenoxy)-8-methyl-9-benzylpurine

Base Information

Chemical Name:2-(3-dimethylaminocarbonylphenoxy)-6-(2-benzyloxy-5-cyanophenoxy)-8-methyl-9-benzylpurine
CAS No.:203925-92-2
Molecular Formula:C₃₆H₃₀N₆O₄
Molecular Weight:610.672
Hs Code.:

Synonyms:2-(3-dimethylaminocarbonylphenoxy)-6-(2-benzyloxy-5-cyanophenoxy)-8-methyl-9-benzylpurine

Suppliers and Price of 2-(3-dimethylaminocarbonylphenoxy)-6-(2-benzyloxy-5-cyanophenoxy)-8-methyl-9-benzylpurine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-(3-dimethylaminocarbonylphenoxy)-6-(2-benzyloxy-5-cyanophenoxy)-8-methyl-9-benzylpurine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-(3-dimethylaminocarbonylphenoxy)-6-(2-benzyloxy-5-cyanophenoxy)-8-methyl-9-benzylpurine

There total 8 articles about 2-(3-dimethylaminocarbonylphenoxy)-6-(2-benzyloxy-5-cyanophenoxy)-8-methyl-9-benzylpurine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 15789-03-4
3-hydroxy-N,N-dimethylbenzamide

: 203925-92-2
2-(3-dimethylaminocarbonylphenoxy)-6-(2-benzyloxy-5-cyanophenoxy)-8-methyl-9-benzylpurine

Guidance literature:: Multi-step reaction with 3 steps

1: 52 percent / Cs₂CO₃ / acetonitrile / 0 °C

2: Zn, 10percent HCl / tetrahydrofuran / 0.5 h / 70 °C

3: 190 °C / 0.5 Torr

With hydrogenchloride; caesium carbonate; zinc; In tetrahydrofuran; acetonitrile;
DOI:10.1016/S0960-894X(98)00386-2

Reference yield:

: 100-46-9
benzylamine

: 203925-92-2
2-(3-dimethylaminocarbonylphenoxy)-6-(2-benzyloxy-5-cyanophenoxy)-8-methyl-9-benzylpurine

Guidance literature:: Multi-step reaction with 5 steps

1: 65 percent / Cs₂CO₃ / acetonitrile / 4 h / 75 °C

2: 95 percent / KHSO₅ / methanol; H₂O

3: 52 percent / Cs₂CO₃ / acetonitrile / 0 °C

4: Zn, 10percent HCl / tetrahydrofuran / 0.5 h / 70 °C

5: 190 °C / 0.5 Torr

With hydrogenchloride; potassium peroxomonosulfate; caesium carbonate; zinc; In tetrahydrofuran; methanol; water; acetonitrile;
DOI:10.1016/S0960-894X(98)00386-2

Reference yield:

: 194985-94-9
3-hydroxy-4-(benzyloxy)benzonitrile

: 203925-92-2
2-(3-dimethylaminocarbonylphenoxy)-6-(2-benzyloxy-5-cyanophenoxy)-8-methyl-9-benzylpurine

Guidance literature:: Multi-step reaction with 6 steps

1: 56 percent / Cs₂CO₃ / acetonitrile / 0 °C

2: 65 percent / Cs₂CO₃ / acetonitrile / 4 h / 75 °C

3: 95 percent / KHSO₅ / methanol; H₂O

4: 52 percent / Cs₂CO₃ / acetonitrile / 0 °C

5: Zn, 10percent HCl / tetrahydrofuran / 0.5 h / 70 °C

6: 190 °C / 0.5 Torr

With hydrogenchloride; potassium peroxomonosulfate; caesium carbonate; zinc; In tetrahydrofuran; methanol; water; acetonitrile;
DOI:10.1016/S0960-894X(98)00386-2