2-methyl-1-(((4-nitrophenoxy)carbonyl)oxy)propyl propionate

Base Information

• Chemical Name: 2-methyl-1-(((4-nitrophenoxy)carbonyl)oxy)propyl propionate
• CAS No.: 1224849-38-0
• Molecular Formula: C₁₄H₁₇NO₇
• Molecular Weight: 311.291
• Mol file: 1224849-38-0.mol

Synonyms:2-methyl-1-(((4-nitrophenoxy)carbonyl)oxy)propyl propionate

Chemical Property of 2-methyl-1-(((4-nitrophenoxy)carbonyl)oxy)propyl propionate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-methyl-1-(((4-nitrophenoxy)carbonyl)oxy)propyl propionate

There total 3 articles about 2-methyl-1-(((4-nitrophenoxy)carbonyl)oxy)propyl propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-iodo-2-methylpropyl 4-nitrophenyl carbonate (1224849-37-9) + silver(1+) propionate (5489-14-5) → 2-methyl-1-(((4-nitrophenoxy)carbonyl)oxy)propyl propionate (1224849-38-0)

Guidance literature:

In toluene; at 90 ℃; for 2h;

Reference yield:

1-chloro-2-methylpropyl(4-nitrophenyl)carbonate (478296-54-7) + propionic acid (802294-64-0,79-09-4) → 2-methyl-1-(((4-nitrophenoxy)carbonyl)oxy)propyl propionate (1224849-38-0)

Guidance literature:

With silver(l) oxide; at 95 ℃; for 1h;

Reference yield:

1-chloro-2-methylpropyl(4-nitrophenyl)carbonate (478296-54-7) → 2-methyl-1-(((4-nitrophenoxy)carbonyl)oxy)propyl propionate (1224849-38-0)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium iodide; calcium chloride / toluene / 9 h / Reflux

2: toluene / 2 h / 90 °C

With sodium iodide; calcium chloride; In toluene;

upstream raw materials:

1-chloro-2-methylpropyl(4-nitrophenyl)carbonate

1-iodo-2-methylpropyl 4-nitrophenyl carbonate

silver⁽¹⁺⁾ propionate

propionic acid

Refernces

• 1、 -. "COMPOUND HAVING TAFIA INHIBITORY ACTIVITY". . . Retrieved 2011/09/20.