(4-methoxyphenyl)methyl 6-deoxy-3-O-<(4-methoxyphenyl)methyl>-4-O-(trimethylsilyl)-β-D-galactopyranoside

Base Information

Chemical Name:(4-methoxyphenyl)methyl 6-deoxy-3-O-<(4-methoxyphenyl)methyl>-4-O-(trimethylsilyl)-β-D-galactopyranoside
CAS No.:168567-27-9
Molecular Formula:C₂₅H₃₆O₇Si
Molecular Weight:476.642
Hs Code.:

Synonyms:(4-methoxyphenyl)methyl 6-deoxy-3-O-<(4-methoxyphenyl)methyl>-4-O-(trimethylsilyl)-β-D-galactopyranoside

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Chemical Property of (4-methoxyphenyl)methyl 6-deoxy-3-O-<(4-methoxyphenyl)methyl>-4-O-(trimethylsilyl)-β-D-galactopyranoside

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Technology Process of (4-methoxyphenyl)methyl 6-deoxy-3-O-<(4-methoxyphenyl)methyl>-4-O-(trimethylsilyl)-β-D-galactopyranoside

There total 5 articles about (4-methoxyphenyl)methyl 6-deoxy-3-O-<(4-methoxyphenyl)methyl>-4-O-(trimethylsilyl)-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75829-69-5
3,4-di-O-acetyl-1,5-anhydro-2,6-dideoxy-D-lyxo-hex-1-enitol

: 168567-27-9
(4-methoxyphenyl)methyl 6-deoxy-3-O-<(4-methoxyphenyl)methyl>-4-O-(trimethylsilyl)-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: MeONa / methanol / 12 h

2: 1.) Bu₂SnO, 2.) CsF / 1.) MeOH, reflux, 1 h, 2.) DMF, 80 deg C, 3 h

3: 1.) dimethyldioxirane / 1.) CH₂Cl₂, acetone, 0 deg C, 30 min, 2.) CH₂Cl₂, acetone, RT, 12 h

4: 1.) pyridine, 2.) K₂CO₃ / 1.) CH₂Cl₂, RT, 15 min, 2.) MeOH, RT, 90 min

With pyridine; sodium methylate; 3,3-dimethyldioxirane; di(n-butyl)tin oxide; potassium carbonate; cesium fluoride; In methanol;
DOI:10.1021/ja00126a013

Reference yield:

: 2746-25-0
p-Methoxybenzyl bromide

: 168567-27-9
(4-methoxyphenyl)methyl 6-deoxy-3-O-<(4-methoxyphenyl)methyl>-4-O-(trimethylsilyl)-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) Bu₂SnO, 2.) CsF / 1.) MeOH, reflux, 1 h, 2.) DMF, 80 deg C, 3 h

2: 1.) dimethyldioxirane / 1.) CH₂Cl₂, acetone, 0 deg C, 30 min, 2.) CH₂Cl₂, acetone, RT, 12 h

3: 1.) pyridine, 2.) K₂CO₃ / 1.) CH₂Cl₂, RT, 15 min, 2.) MeOH, RT, 90 min

With pyridine; 3,3-dimethyldioxirane; di(n-butyl)tin oxide; potassium carbonate; cesium fluoride;
DOI:10.1021/ja00126a013

Reference yield:

: 134355-03-6
6-deoxy-D-glucal

: 168567-27-9
(4-methoxyphenyl)methyl 6-deoxy-3-O-<(4-methoxyphenyl)methyl>-4-O-(trimethylsilyl)-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) Bu₂SnO, 2.) CsF / 1.) MeOH, reflux, 1 h, 2.) DMF, 80 deg C, 3 h

2: 1.) dimethyldioxirane / 1.) CH₂Cl₂, acetone, 0 deg C, 30 min, 2.) CH₂Cl₂, acetone, RT, 12 h

3: 1.) pyridine, 2.) K₂CO₃ / 1.) CH₂Cl₂, RT, 15 min, 2.) MeOH, RT, 90 min

With pyridine; 3,3-dimethyldioxirane; di(n-butyl)tin oxide; potassium carbonate; cesium fluoride;
DOI:10.1021/ja00126a013