1-naphthalene-2,2,2-trifluoro-1-<4-(1-triphenylmethyl)imidazole>ethyl phenyl thionocarbonate

Base Information

• Chemical Name: 1-naphthalene-2,2,2-trifluoro-1-<4-(1-triphenylmethyl)imidazole>ethyl phenyl thionocarbonate
• CAS No.: 161530-07-0
• Molecular Formula: C₄₁H₂₉F₃N₂O₂S
• Molecular Weight: 670.755
• Mol file: 161530-07-0.mol

Synonyms:1-naphthalene-2,2,2-trifluoro-1-<4-(1-triphenylmethyl)imidazole>ethyl phenyl thionocarbonate

Chemical Property of 1-naphthalene-2,2,2-trifluoro-1-<4-(1-triphenylmethyl)imidazole>ethyl phenyl thionocarbonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-naphthalene-2,2,2-trifluoro-1-<4-(1-triphenylmethyl)imidazole>ethyl phenyl thionocarbonate

There total 1 articles about 1-naphthalene-2,2,2-trifluoro-1-<4-(1-triphenylmethyl)imidazole>ethyl phenyl thionocarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

4-<(1-naphthyl)(trifluoromethyl)hydroxymethyl>-N-(triphenylmethyl)imidazole (156833-35-1) + phenylcarbonochloridothioate (1005-56-7) → 1-naphthalene-2,2,2-trifluoro-1-<4-(1-triphenylmethyl)imidazole>ethyl phenyl thionocarbonate (161530-07-0)

Guidance literature:

With pyridine; In dichloromethane; for 16h; Ambient temperature;

DOI:10.3987/COM-94-S(B)77

Reference yield:

1-naphthalene-2,2,2-trifluoro-1-<4-(1-triphenylmethyl)imidazole>ethyl phenyl thionocarbonate (161530-07-0) → 4-<1-(1-naphthalenyl)-2,2,2-trifluoroethyl>-<1-(triphenylmethyl)>imidazole

Guidance literature:

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; at 75 - 80 ℃; for 3h; Yield given;

DOI:10.3987/COM-94-S(B)77

upstream raw materials:

4-<(1-naphthyl)(trifluoromethyl)hydroxymethyl>-N-(triphenylmethyl)imidazole

phenylcarbonochloridothioate