4-(1-Methyl-3-phenyl-2-propinyliden)morpholinium-trifluormethansulfonat

Base Information

• Chemical Name: 4-(1-Methyl-3-phenyl-2-propinyliden)morpholinium-trifluormethansulfonat
• CAS No.: 115018-07-0
• Molecular Formula: CF₃O₃S*C₁₄H₁₆NO
• Molecular Weight: 363.358

Synonyms:4-(1-Methyl-3-phenyl-2-propinyliden)morpholinium-trifluormethansulfonat

Chemical Property of 4-(1-Methyl-3-phenyl-2-propinyliden)morpholinium-trifluormethansulfonat

Chemical Property:

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Technology Process of 4-(1-Methyl-3-phenyl-2-propinyliden)morpholinium-trifluormethansulfonat

There total 1 articles about 4-(1-Methyl-3-phenyl-2-propinyliden)morpholinium-trifluormethansulfonat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

4-(1-Methyl-3-phenyl-3-trifluoromethylsulfonyloxy-2-propenylidene)morpholinium trifluoromethanesulfonate (109123-43-5) → 4-(1-Methyl-3-phenyl-2-propinyliden)morpholinium-trifluormethansulfonat (115018-07-0)

Guidance literature:

In acetonitrile; for 24h; Heating;

Reference yield: 77.0%

tri-tert-butylazete (103794-87-2) + 4-(1-Methyl-3-phenyl-2-propinyliden)morpholinium-trifluormethansulfonat (115018-07-0) → 4-(6,7,8-tri-tert-butyl-2-phenyl-1-azabicyclo<4.2.0>octa-2,7-dien-4-ylidene)morpholinium trifluoromethanesulfonate

Guidance literature:

In dichloromethane; 1.) -78 deg C, 30 min, 2.) -78 deg C to r.t.;

Reference yield: 68.0%

1,3-diphenylisobenzofuran (5471-63-6) + 4-(1-Methyl-3-phenyl-2-propinyliden)morpholinium-trifluormethansulfonat (115018-07-0) → 4-<1-(1,4-Dihydro-1,3,4-triphenyl-1,4-epoxy-2-naphthyl)ethyliden>morpholinium-trifluormethansulfonat (115018-25-2)

Guidance literature:

for 3h; Ambient temperature;

upstream raw materials:

4-(1-Methyl-3-phenyl-3-trifluoromethylsulfonyloxy-2-propenylidene)morpholinium trifluoromethanesulfonate

Downstream raw materials:

4-(1-Methyl-3-morpholino-3-phenyl-2-propenyliden)morpholinium-trifluormethansulfonat

11-Acetyl-9,10-dihydro-12-phenyl-9,10-ethenoanthracen

4-<1-(1,4-Dihydro-1,3,4-triphenyl-1,4-epoxy-2-naphthyl)ethyliden>morpholinium-trifluormethansulfonat

2-morpholino-4,4-diphenyl-1,3-butadiene

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