6-(benzoyloxy)-3-hydroxy-2-methylenehexanoic acid, methyl ester

Base Information

• Chemical Name: 6-(benzoyloxy)-3-hydroxy-2-methylenehexanoic acid, methyl ester
• CAS No.: 87050-30-4
• Molecular Formula: C₁₅H₁₈O₅
• Molecular Weight: 278.305
• Mol file: 87050-30-4.mol

Synonyms:6-(benzoyloxy)-3-hydroxy-2-methylenehexanoic acid, methyl ester

Chemical Property of 6-(benzoyloxy)-3-hydroxy-2-methylenehexanoic acid, methyl ester

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 6-(benzoyloxy)-3-hydroxy-2-methylenehexanoic acid, methyl ester

There total 1 articles about 6-(benzoyloxy)-3-hydroxy-2-methylenehexanoic acid, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

4-oxobutyl benzoate (22927-31-7) + acrylic acid methyl ester (292638-85-8,9003-21-8,96-33-3) → 6-(benzoyloxy)-3-hydroxy-2-methylenehexanoic acid, methyl ester (87050-30-4)

Guidance literature:

With 1,4-diaza-bicyclo[2.2.2]octane; for 168h; Ambient temperature;

DOI:10.1021/jo00220a034

Reference yield: 95.0%

6-(benzoyloxy)-3-hydroxy-2-methylenehexanoic acid, methyl ester (87050-30-4) → 6-(benzoyloxy)-2-(bromomethyl)-2-hexenoic acid, methyl ester (87050-32-6)

Guidance literature:

With N-Bromosuccinimide; dimethylsulfide; In dichloromethane; for 24h; Ambient temperature;

DOI:10.1021/jo00220a034

upstream raw materials:

4-oxobutyl benzoate

acrylic acid methyl ester

Downstream raw materials:

6-(benzoyloxy)-2-(bromomethyl)-2-hexenoic acid, methyl ester