1α,3β,4β-trihydroxy-5α-{[3-(3-hydroxy-4-methoxyphenyl)propanoyl]oxy}cyclohexane-β-carboxylic acid

Base Information

Chemical Name:1α,3β,4β-trihydroxy-5α-{[3-(3-hydroxy-4-methoxyphenyl)propanoyl]oxy}cyclohexane-β-carboxylic acid
CAS No.:27782-99-6
Molecular Formula:C₁₇H₂₂O₉
Molecular Weight:370.356
Hs Code.:

Synonyms:1α,3β,4β-trihydroxy-5α-{[3-(3-hydroxy-4-methoxyphenyl)propanoyl]oxy}cyclohexane-β-carboxylic acid

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Chemical Property of 1α,3β,4β-trihydroxy-5α-{[3-(3-hydroxy-4-methoxyphenyl)propanoyl]oxy}cyclohexane-β-carboxylic acid

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Technology Process of 1α,3β,4β-trihydroxy-5α-{[3-(3-hydroxy-4-methoxyphenyl)propanoyl]oxy}cyclohexane-β-carboxylic acid

There total 3 articles about 1α,3β,4β-trihydroxy-5α-{[3-(3-hydroxy-4-methoxyphenyl)propanoyl]oxy}cyclohexane-β-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 76799-19-4
benzyl 1α,3β,4β-trihydroxy-5α-<<3-(3-hydroxy-4-methoxyphenyl)propenoyl>oxy>cyclohexane-β-carboxylate

: 27782-99-6
1α,3β,4β-trihydroxy-5α-{[3-(3-hydroxy-4-methoxyphenyl)propanoyl]oxy}cyclohexane-β-carboxylic acid

Guidance literature:: With hydrogen; palladium on activated charcoal; In tetrahydrofuran; for 96h; under 760 Torr; Ambient temperature;
DOI:10.1021/jm00136a011

Reference yield:

: 202650-88-2
3-caffeoylquinic acid

: 27782-99-6
1α,3β,4β-trihydroxy-5α-{[3-(3-hydroxy-4-methoxyphenyl)propanoyl]oxy}cyclohexane-β-carboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 38 percent / K₂CO₃ / dimethylformamide / 144 h / Ambient temperature

2: 42 percent / K₂CO₃ / dimethylformamide / 18 h / Ambient temperature

3: 38 percent / H₂ / Pd/C / tetrahydrofuran / 96 h / 760 Torr / Ambient temperature

With hydrogen; potassium carbonate; palladium on activated charcoal; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jm00136a011

Reference yield:

: 76820-10-5
benzyl chlorogenate

: 27782-99-6
1α,3β,4β-trihydroxy-5α-{[3-(3-hydroxy-4-methoxyphenyl)propanoyl]oxy}cyclohexane-β-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 42 percent / K₂CO₃ / dimethylformamide / 18 h / Ambient temperature

2: 38 percent / H₂ / Pd/C / tetrahydrofuran / 96 h / 760 Torr / Ambient temperature

With hydrogen; potassium carbonate; palladium on activated charcoal; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jm00136a011