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Technology Process of NH3CHCH2C6H4OHCONHCH2CONHCH2CONHCHCH2C6H5CONHCHCOOCH2CH(CH3)2Co(NH3)5(3+)*3CF3COO(1-)

NH3CHCH2C6H4OHCONHCH2CONHCH2CONHCHCH2C6H5CONHCHCOOCH2CH(CH3)2Co(NH3)5(3+)*3CF3COO(1-)

Base Information
  • Chemical Name:NH3CHCH2C6H4OHCONHCH2CONHCH2CONHCHCH2C6H5CONHCHCOOCH2CH(CH3)2Co(NH3)5(3+)*3CF3COO(1-)
  • CAS No.:81688-63-3
  • Molecular Formula:3C2F3O2*C28H52CoN10O7
  • Molecular Weight:1038.82
  • Hs Code.:
NH<sub>3</sub>CHCH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>OHCONHCH<sub>2</sub>CONHCH<sub>2</sub>CONHCHCH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>CONHCHCOOCH<sub>2</sub>CH(CH<sub>3</sub>)2Co(NH<sub>3</sub>)5<sup>(3+)</sup>*3CF<sub>3</sub>COO<sup>(1-)</sup>

Synonyms:NH3CHCH2C6H4OHCONHCH2CONHCH2CONHCHCH2C6H5CONHCHCOOCH2CH(CH3)2Co(NH3)5(3+)*3CF3COO(1-)

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Chemical Property of NH3CHCH2C6H4OHCONHCH2CONHCH2CONHCHCH2C6H5CONHCHCOOCH2CH(CH3)2Co(NH3)5(3+)*3CF3COO(1-)
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Technology Process of NH3CHCH2C6H4OHCONHCH2CONHCH2CONHCHCH2C6H5CONHCHCOOCH2CH(CH3)2Co(NH3)5(3+)*3CF3COO(1-)

There total 1 articles about NH3CHCH2C6H4OHCONHCH2CONHCH2CONHCHCH2C6H5CONHCHCOOCH2CH(CH3)2Co(NH3)5(3+)*3CF3COO(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

NH<sub>3</sub>CH<sub>2</sub>CONHCH<sub>2</sub>CONHCHCH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>CONHCHCOOCH<sub>2</sub>CH(CH<sub>3</sub>)2Co(NH<sub>3</sub>)5<sup>(3+)</sup>*3CF<sub>3</sub>COO<sup>(1-)</sup>
81688-60-0

NH3CH2CONHCH2CONHCHCH2C6H5CONHCHCOOCH2CH(CH3)2Co(NH3)5(3+)*3CF3COO(1-)

Leu-enkephalin
58822-25-6

Leu-enkephalin

trifluoroacetic acid
76-05-1

trifluoroacetic acid

NH<sub>3</sub>CHCH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>OHCONHCH<sub>2</sub>CONHCH<sub>2</sub>CONHCHCH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>CONHCHCOOCH<sub>2</sub>CH(CH<sub>3</sub>)2Co(NH<sub>3</sub>)5<sup>(3+)</sup>*3CF<sub>3</sub>COO<sup>(1-)</sup>
81688-63-3

NH3CHCH2C6H4OHCONHCH2CONHCH2CONHCHCH2C6H5CONHCHCOOCH2CH(CH3)2Co(NH3)5(3+)*3CF3COO(1-)

Guidance literature:
With sodium hydrogencarbonate; In tetrahydrofuran; 1,4-dioxane; water; Co-complex was dissolved in H2O, pH was adjusted to 8 with NaHCO3, BocTyrOSu in THF and dioxane was added, mixt. was left stirring at room temp. for 24 h, concd. on rotary evaporator, CF3COOH was added, stirred for 1.5 h; evapd. to dryness by rotary evaporator, purified by column chromy. withMeOH-H2O HOAc, soln. was evapd. to dryness;
DOI:10.1021/ja00378a021
upstream raw materials:

NH3CH2CONHCH2CONHCHCH2C6H5CONHCHCOOCH2CH(CH3)2Co(NH3)5(3+)*3CF3COO(1-)

Leu-enkephalin

trifluoroacetic acid

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