5-(4-ethynylphenyl)-10,15,20-tris-(3,5-dimethoxyphenyl)porphyrinato zinc (II)

Base Information

Chemical Name:5-(4-ethynylphenyl)-10,15,20-tris-(3,5-dimethoxyphenyl)porphyrinato zinc (II)
CAS No.:1094159-89-3
Molecular Formula:C₅₂H₄₀N₄O₆Zn
Molecular Weight:882.303
Hs Code.:

Synonyms:5-(4-ethynylphenyl)-10,15,20-tris-(3,5-dimethoxyphenyl)porphyrinato zinc (II)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-(4-ethynylphenyl)-10,15,20-tris-(3,5-dimethoxyphenyl)porphyrinato zinc (II)

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Technology Process of 5-(4-ethynylphenyl)-10,15,20-tris-(3,5-dimethoxyphenyl)porphyrinato zinc (II)

There total 4 articles about 5-(4-ethynylphenyl)-10,15,20-tris-(3,5-dimethoxyphenyl)porphyrinato zinc (II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1094159-88-2
5-(4-(trimethylsilylethynyl)-phenyl)-10,15,20-tri(3,5-dimethoxy-phenyl)-porphyrinatozinc(II)

: 1094159-89-3
5-(4-ethynylphenyl)-10,15,20-tris-(3,5-dimethoxyphenyl)porphyrinato zinc (II)

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 2h;
DOI:10.1016/j.tet.2008.08.054

Reference yield:

: 77123-57-0
4-[(trimethylsilyl)ethynyl]bezaldehyde

: 1094159-89-3
5-(4-ethynylphenyl)-10,15,20-tris-(3,5-dimethoxyphenyl)porphyrinato zinc (II)

Guidance literature:: Multi-step reaction with 3 steps

1: trifluoroacetic acid / chloroform

2: tetrahydrofuran

3: tetrabutyl ammonium fluoride / tetrahydrofuran

With tetrabutyl ammonium fluoride; trifluoroacetic acid; In tetrahydrofuran; chloroform;
DOI:10.1002/chem.202004928

Reference yield:

: C₅₅H₅₀N₄O₆Si

: 1094159-89-3
5-(4-ethynylphenyl)-10,15,20-tris-(3,5-dimethoxyphenyl)porphyrinato zinc (II)

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran

2: tetrabutyl ammonium fluoride / tetrahydrofuran

With tetrabutyl ammonium fluoride; In tetrahydrofuran;
DOI:10.1002/chem.202004928