methyl 6-O-(3-O-allyl-2,4-di-O-benzoyl-β-D-glucopyranosyl)-2,3,4-tri-O-benzoyl-α-D-glucopyranoside

Base Information

• Chemical Name: methyl 6-O-(3-O-allyl-2,4-di-O-benzoyl-β-D-glucopyranosyl)-2,3,4-tri-O-benzoyl-α-D-glucopyranoside
• CAS No.: 1029884-27-2
• Molecular Formula: C₅₁H₄₈O₁₆
• Molecular Weight: 916.933

Synonyms:methyl 6-O-(3-O-allyl-2,4-di-O-benzoyl-β-D-glucopyranosyl)-2,3,4-tri-O-benzoyl-α-D-glucopyranoside

Chemical Property of methyl 6-O-(3-O-allyl-2,4-di-O-benzoyl-β-D-glucopyranosyl)-2,3,4-tri-O-benzoyl-α-D-glucopyranoside

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Technology Process of methyl 6-O-(3-O-allyl-2,4-di-O-benzoyl-β-D-glucopyranosyl)-2,3,4-tri-O-benzoyl-α-D-glucopyranoside

There total 1 articles about methyl 6-O-(3-O-allyl-2,4-di-O-benzoyl-β-D-glucopyranosyl)-2,3,4-tri-O-benzoyl-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C53H49ClO17 → methyl 6-O-(3-O-allyl-2,4-di-O-benzoyl-β-D-glucopyranosyl)-2,3,4-tri-O-benzoyl-α-D-glucopyranoside (1029884-27-2)

Guidance literature:

With pyridine; water; at 50 ℃;

DOI:10.1039/b800809d

Reference yield: 88.0%

methyl 6-O-(3-O-allyl-2,4-di-O-benzoyl-β-D-glucopyranosyl)-2,3,4-tri-O-benzoyl-α-D-glucopyranoside (1029884-27-2) + dodecyl 2,3,4,6-tetra-O-benzoyl-1-thio-β-D-glucopyranoside (275817-34-0) → C85H74O25 (1029884-31-8)

Guidance literature:

methyl 6-O-(3-O-allyl-2,4-di-O-benzoyl-β-D-glucopyranosyl)-2,3,4-tri-O-benzoyl-α-D-glucopyranoside; dodecyl 2,3,4,6-tetra-O-benzoyl-1-thio-β-D-glucopyranoside; With N-iodo-succinimide; In dichloromethane; for 0.5h; Molecular sieve; Inert atmosphere;

With trifluorormethanesulfonic acid; In dichloromethane; at -20 - 20 ℃;

DOI:10.1039/b800809d

Reference yield:

dodecyl 2,3,4-tri-O-benzoyl-6-O-chloroacetyl-1-thio-β-D-glucopyranoside (1029884-22-7) + methyl 6-O-(3-O-allyl-2,4-di-O-benzoyl-β-D-glucopyranosyl)-2,3,4-tri-O-benzoyl-α-D-glucopyranoside (1029884-27-2) → C80H71ClO25

Guidance literature:

dodecyl 2,3,4-tri-O-benzoyl-6-O-chloroacetyl-1-thio-β-D-glucopyranoside; methyl 6-O-(3-O-allyl-2,4-di-O-benzoyl-β-D-glucopyranosyl)-2,3,4-tri-O-benzoyl-α-D-glucopyranoside; With N-iodo-succinimide; In dichloromethane; for 0.5h; Molecular sieve; Inert atmosphere;

With trifluorormethanesulfonic acid; In dichloromethane; at -20 - 20 ℃;

DOI:10.1039/b800809d

Downstream raw materials:

C₈₅H₇₄O₂₅

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