L-β-hydroxy-N-methylvaline

Base Information

• Chemical Name: L-β-hydroxy-N-methylvaline
• CAS No.: 77421-34-2
• Molecular Formula: C₆H₁₃NO₃
• Molecular Weight: 147.174
• Mol file: 77421-34-2.mol

Synonyms:L-β-hydroxy-N-methylvaline

Chemical Property of L-β-hydroxy-N-methylvaline

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of L-β-hydroxy-N-methylvaline

There total 2 articles about L-β-hydroxy-N-methylvaline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

luzopeptin C (76110-01-5) → sarcosine (107-97-1,25951-24-0) + D-Serine (312-84-5,83245-15-2) + L-β-hydroxy-N-methylvaline (77421-34-2) + glycine (56-40-6,18875-39-3,25718-94-9)

Guidance literature:

With hydrogenchloride; at 100 ℃; for 18h; Further byproducts given;

DOI:10.1021/ja00395a054

Reference yield:

(S)-3-Hydroxy-3-methyl-2-methylamino-butyric acid (R)-2-(carboxymethyl-methyl-carbamoyl)-2-[(3-hydroxy-6-methoxy-quinoline-2-carbonyl)-amino]-ethyl ester → sarcosine (107-97-1,25951-24-0) + L-β-hydroxy-N-methylvaline (77421-34-2) + (R)-3-Hydroxy-2-[(3-hydroxy-6-methoxy-quinoline-2-carbonyl)-amino]-propionic acid (77431-62-0)

Guidance literature:

With water; hydroxide;

DOI:10.1021/ja00395a054

upstream raw materials:

luzopeptin C