4-METHOXYPHENYL 3-O-ALLYL-2-AZIDO-4,6-O-BENZYLIDENE-2-DEOXY-BETA-D-GLUCOPYRANOSIDE

Base Information

• Chemical Name: 4-METHOXYPHENYL 3-O-ALLYL-2-AZIDO-4,6-O-BENZYLIDENE-2-DEOXY-BETA-D-GLUCOPYRANOSIDE
• CAS No.: 889453-78-5
• Molecular Formula: C₂₃H₂₅N₃O₆
• Molecular Weight: 439.468
• Mol file: 889453-78-5.mol

Synonyms:b-D-Glucopyranoside,4-methoxyphenyl 2-azido-2-deoxy-4,6-O-(phenylmethylene)-3-O-2-propenyl- (9CI)

Chemical Property of 4-METHOXYPHENYL 3-O-ALLYL-2-AZIDO-4,6-O-BENZYLIDENE-2-DEOXY-BETA-D-GLUCOPYRANOSIDE

Chemical Property:

• Melting Point: 119.0 to 123.0 °C
• Storage Temp.: Freezer

Purity/Quality:

98%,99%, ^*data from raw suppliers

4-Methoxyphenyl 3-O-Allyl-2-azido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-METHOXYPHENYL 3-O-ALLYL-2-AZIDO-4,6-O-BENZYLIDENE-2-DEOXY-BETA-D-GLUCOPYRANOSIDE

There total 2 articles about 4-METHOXYPHENYL 3-O-ALLYL-2-AZIDO-4,6-O-BENZYLIDENE-2-DEOXY-BETA-D-GLUCOPYRANOSIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

allyl bromide (106-95-6) + 4-methoxyphenyl 2-azido-4,6-O-benzylidene-2-deoxy-α-D-galactopyranoside (165397-91-1,1340541-47-0) → C23H25N3O6 (889453-78-5)

Guidance literature:

With tetrabutylammomium bromide; sodium hydroxide; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

DOI:10.1016/j.tet.2019.130697

Reference yield:

p-methoxyphenyl 2-azido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside (1430068-18-0,1340541-47-0) + allyl bromide (106-95-6) → C23H25N3O6 (889453-78-5)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; for 2h;

DOI:10.1016/j.tet.2020.131412

upstream raw materials:

allyl bromide

4-methoxyphenyl 2-azido-4,6-O-benzylidene-2-deoxy-α-D-galactopyranoside

p-methoxyphenyl 2-azido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

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