1,1’-((2,3,5,6-tetramethyl-1,4-phenylene)bis(methylene))bis(1H-imidazole)

Base Information

• Chemical Name: 1,1’-((2,3,5,6-tetramethyl-1,4-phenylene)bis(methylene))bis(1H-imidazole)
• CAS No.: 1012075-54-5
• Molecular Formula: C₁₈H₂₂N₄
• Molecular Weight: 294.399

Synonyms:1,1’-((2,3,5,6-tetramethyl-1,4-phenylene)bis(methylene))bis(1H-imidazole)

Chemical Property of 1,1’-((2,3,5,6-tetramethyl-1,4-phenylene)bis(methylene))bis(1H-imidazole)

Chemical Property:

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Technology Process of 1,1’-((2,3,5,6-tetramethyl-1,4-phenylene)bis(methylene))bis(1H-imidazole)

There total 1 articles about 1,1’-((2,3,5,6-tetramethyl-1,4-phenylene)bis(methylene))bis(1H-imidazole) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

1H-imidazole (288-32-4) + 1,4-bis(bromomethyl)-2,3,5,6-tetramethylbenzene (35168-64-0) → 1,1’-((2,3,5,6-tetramethyl-1,4-phenylene)bis(methylene))bis(1H-imidazole) (1012075-54-5)

Guidance literature:

In methanol; at 65 ℃; for 16h;

DOI:10.1021/ic400315g

Reference yield: 88.0%

copper (II) carbonate hydroxide + carbon dioxide (124-38-9,18923-20-1) + water (7732-18-5) + 1,1’-((2,3,5,6-tetramethyl-1,4-phenylene)bis(methylene))bis(1H-imidazole) (1012075-54-5) → {[Cu(CO3)(1,4-bis(imidazol-1-ylmethyl)-2,3,5,6-tetramethylbenzene)]·2H2O}n

Guidance literature:

With ammonium hydroxide; In ethanol; at 20 ℃;

DOI:10.1021/ic400315g

Reference yield: 82.0%

carbon dioxide (124-38-9,18923-20-1) + water (7732-18-5) + copper hydroxide (20427-59-2) + 1,1’-((2,3,5,6-tetramethyl-1,4-phenylene)bis(methylene))bis(1H-imidazole) (1012075-54-5) → {[Cu(CO3)(1,4-bis(imidazol-1-ylmethyl)-2,3,5,6-tetramethylbenzene)]·2H2O}n

Guidance literature:

With ammonium hydroxide; In ethanol; at 20 ℃;

DOI:10.1021/ic400315g

upstream raw materials:

1H-imidazole

1,4-bis(bromomethyl)-2,3,5,6-tetramethylbenzene

Downstream raw materials:

C₃₆H₄₄CuN₈O₈S₂^(2-)*C₃₆H₄₈CuN₈O₂⁽²⁺⁾

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