(+/-)-2,7,12-trimethoxy-3,8,13-tris<(2-phenyltetrazolyl)oxy>-10,15-dihydro-5H-tribenzocyclononene

Base Information

Chemical Name:(+/-)-2,7,12-trimethoxy-3,8,13-tris<(2-phenyltetrazolyl)oxy>-10,15-dihydro-5H-tribenzocyclononene
CAS No.:89209-32-5
Molecular Formula:C₄₅H₃₆N₁₂O₆
Molecular Weight:840.858
Hs Code.:

(+/-)-2,7,12-trimethoxy-3,8,13-tris<(2-phenyltetrazolyl)oxy>-10,15-dihydro-5H-tribenzo<a,d,g>cyclononene

Synonyms:(+/-)-2,7,12-trimethoxy-3,8,13-tris<(2-phenyltetrazolyl)oxy>-10,15-dihydro-5H-tribenzocyclononene

Suppliers and Price of (+/-)-2,7,12-trimethoxy-3,8,13-tris<(2-phenyltetrazolyl)oxy>-10,15-dihydro-5H-tribenzocyclononene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (+/-)-2,7,12-trimethoxy-3,8,13-tris<(2-phenyltetrazolyl)oxy>-10,15-dihydro-5H-tribenzocyclononene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (+/-)-2,7,12-trimethoxy-3,8,13-tris<(2-phenyltetrazolyl)oxy>-10,15-dihydro-5H-tribenzocyclononene

There total 2 articles about (+/-)-2,7,12-trimethoxy-3,8,13-tris<(2-phenyltetrazolyl)oxy>-10,15-dihydro-5H-tribenzocyclononene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 14210-25-4
5-Chloro-1-phenyltetrazole

: 81370-49-2,68198-62-9,75322-24-6,68182-93-4
cyclotriguaiacyclene

: 89209-32-5
(+/-)-2,7,12-trimethoxy-3,8,13-tris<(2-phenyltetrazolyl)oxy>-10,15-dihydro-5H-tribenzocyclononene

Guidance literature:: With potassium tert-butylate; In N,N-dimethyl-formamide;

Reference yield:

: 86534-12-5,123805-89-0,123805-90-3
(±)-2,7,12-trimethoxy-3,8,13-tris(2-propenyloxy)-10,15-dihydro-5Htribenzo[a,d,g]cyclononene

: 89209-32-5
(+/-)-2,7,12-trimethoxy-3,8,13-tris<(2-phenyltetrazolyl)oxy>-10,15-dihydro-5H-tribenzocyclononene

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / 65percent HClO₄ / 10percent Pd/charcoal / dioxane; ethanol / 20 h / 55 - 60 °C

2: 90 percent / 1) tert-BuOK / dimethylformamide / 1) 10 min, 2) 1 h

With perchloric acid; potassium tert-butylate; palladium on activated charcoal; In 1,4-dioxane; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/ja00332a042

Reference yield:

: 89209-32-5
(+/-)-2,7,12-trimethoxy-3,8,13-tris<(2-phenyltetrazolyl)oxy>-10,15-dihydro-5H-tribenzocyclononene

: 91796-58-6
(+/-)-2,7,12-tris<(-2-phenyl-1-tetrazolyl)oxy>-10,15-dihydro-5H-tribenzocyclononene

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / H₂ / 10percent Pd/C / CH₂Cl₂; methanol / 20 h / 15 - 20 °C / 760 Torr

2: 90 percent / BBr₃ / CH₂Cl₂ / 0 - 20 °C

3: tBuOK / dimethylformamide

With potassium tert-butylate; hydrogen; boron tribromide; palladium on activated charcoal; In methanol; dichloromethane; N,N-dimethyl-formamide;