Cyclohexyl-[1-{3,4,5-trimethoxy-2-[6-(2-methyl-[1,3]oxathiolan-2-yl)-benzo[1,3]dioxol-5-yl]-phenyl}-meth-(Z)-ylidene]-amine

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Chemical Name:Cyclohexyl-[1-{3,4,5-trimethoxy-2-[6-(2-methyl-[1,3]oxathiolan-2-yl)-benzo[1,3]dioxol-5-yl]-phenyl}-meth-(Z)-ylidene]-amine
CAS No.:69174-44-3
Molecular Formula:C₂₇H₃₃NO₆S
Molecular Weight:499.628
Hs Code.:

Synonyms:Cyclohexyl-[1-{3,4,5-trimethoxy-2-[6-(2-methyl-[1,3]oxathiolan-2-yl)-benzo[1,3]dioxol-5-yl]-phenyl}-meth-(Z)-ylidene]-amine

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Chemical Property of Cyclohexyl-[1-{3,4,5-trimethoxy-2-[6-(2-methyl-[1,3]oxathiolan-2-yl)-benzo[1,3]dioxol-5-yl]-phenyl}-meth-(Z)-ylidene]-amine

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Technology Process of Cyclohexyl-[1-{3,4,5-trimethoxy-2-[6-(2-methyl-[1,3]oxathiolan-2-yl)-benzo[1,3]dioxol-5-yl]-phenyl}-meth-(Z)-ylidene]-amine

There total 5 articles about Cyclohexyl-[1-{3,4,5-trimethoxy-2-[6-(2-methyl-[1,3]oxathiolan-2-yl)-benzo[1,3]dioxol-5-yl]-phenyl}-meth-(Z)-ylidene]-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 15930-53-7
6-bromo-3,4-methylenedioxybenzaldehyde

: 69174-44-3
Cyclohexyl-[1-{3,4,5-trimethoxy-2-[6-(2-methyl-[1,3]oxathiolan-2-yl)-benzo[1,3]dioxol-5-yl]-phenyl}-meth-(Z)-ylidene]-amine

Guidance literature:: Multi-step reaction with 4 steps

1: 41.0 g / diethyl ether; tetrahydrofuran / 18 h / 25 °C

2: 64 percent / Jones reagent / acetone / 0.5 h / 5 °C

3: p-TsOH*H₂O / benzene / 3 h / Heating

4: 1.) n-BuLi, 2.) CuI*P(OEt)3

With n-butyllithium; jones reagent; triethylphosphite copper(I) iodide complex; toluene-4-sulfonic acid; In tetrahydrofuran; diethyl ether; acetone; benzene;
DOI:10.1021/ja00522a058

Reference yield:

: 71095-27-7
1-(2′-bromo-4′,5′-methylenedioxyphenyl)ethan-1-ol

: 69174-44-3
Cyclohexyl-[1-{3,4,5-trimethoxy-2-[6-(2-methyl-[1,3]oxathiolan-2-yl)-benzo[1,3]dioxol-5-yl]-phenyl}-meth-(Z)-ylidene]-amine

Guidance literature:: Multi-step reaction with 3 steps

1: 64 percent / Jones reagent / acetone / 0.5 h / 5 °C

2: p-TsOH*H₂O / benzene / 3 h / Heating

3: 1.) n-BuLi, 2.) CuI*P(OEt)3

With n-butyllithium; jones reagent; triethylphosphite copper(I) iodide complex; toluene-4-sulfonic acid; In acetone; benzene;
DOI:10.1021/ja00522a058

Reference yield:

: 71095-26-6
1-(2′-bromo-4′,5′-methylenedioxyphenyl)ethan-1-one

: 69174-44-3
Cyclohexyl-[1-{3,4,5-trimethoxy-2-[6-(2-methyl-[1,3]oxathiolan-2-yl)-benzo[1,3]dioxol-5-yl]-phenyl}-meth-(Z)-ylidene]-amine

Guidance literature:: Multi-step reaction with 2 steps

1: p-TsOH*H₂O / benzene / 3 h / Heating

2: 1.) n-BuLi, 2.) CuI*P(OEt)3

With n-butyllithium; triethylphosphite copper(I) iodide complex; toluene-4-sulfonic acid; In benzene;
DOI:10.1021/ja00522a058