1-benzyl-3-(1-cyclopent-3-enyl-1H-indol-3-yl)-4-(1H-indol-3-yl)-pyrrole-2,5-dione

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Chemical Name:1-benzyl-3-(1-cyclopent-3-enyl-1H-indol-3-yl)-4-(1H-indol-3-yl)-pyrrole-2,5-dione
CAS No.:797055-96-0
Molecular Formula:C₃₂H₂₅N₃O₂
Molecular Weight:483.569
Hs Code.:

Synonyms:1-benzyl-3-(1-cyclopent-3-enyl-1H-indol-3-yl)-4-(1H-indol-3-yl)-pyrrole-2,5-dione

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Chemical Property of 1-benzyl-3-(1-cyclopent-3-enyl-1H-indol-3-yl)-4-(1H-indol-3-yl)-pyrrole-2,5-dione

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Technology Process of 1-benzyl-3-(1-cyclopent-3-enyl-1H-indol-3-yl)-4-(1H-indol-3-yl)-pyrrole-2,5-dione

There total 3 articles about 1-benzyl-3-(1-cyclopent-3-enyl-1H-indol-3-yl)-4-(1H-indol-3-yl)-pyrrole-2,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 91026-01-6
2,3-bis(1H-indol-3-yl)-N-benzylmaleimide

: 253680-54-5
methanesulfonic acid cyclopent-3-enyl ester

: 797055-96-0
1-benzyl-3-(1-cyclopent-3-enyl-1H-indol-3-yl)-4-(1H-indol-3-yl)-pyrrole-2,5-dione

: 797055-94-8
1-benzyl-3,4-bis-(1-but-3-enyl-1H-indol-3-yl)-pyrrole-2,5-dione

Guidance literature:: 2,3-bis(1H-indol-3-yl)-N-benzylmaleimide; With tetra-(n-butyl)ammonium iodide; caesium carbonate; In N,N-dimethyl-formamide; at 23 ℃; for 1h;

methanesulfonic acid cyclopent-3-enyl ester; In N,N-dimethyl-formamide; at 52 ℃; for 96h;
DOI:10.1039/b405010j

Reference yield:

: 120-72-9
indole

: 797055-96-0
1-benzyl-3-(1-cyclopent-3-enyl-1H-indol-3-yl)-4-(1H-indol-3-yl)-pyrrole-2,5-dione

Guidance literature:: Multi-step reaction with 2 steps

1.1: EtMgBr / tetrahydrofuran; diethyl ether; toluene / Heating

1.2: 67 percent / tetrahydrofuran; diethyl ether; toluene / Heating

2.1: Cs₂CO₃; Bu₄NI / dimethylformamide / 1 h / 23 °C

2.2: 36 percent / dimethylformamide / 96 h / 52 °C

With ethylmagnesium bromide; tetra-(n-butyl)ammonium iodide; caesium carbonate; In tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide; toluene;
DOI:10.1039/b405010j

Reference yield:

: 16114-24-2
1-benzyl-3,4-dichloro-pyrrole-2,5-dione

: 797055-96-0
1-benzyl-3-(1-cyclopent-3-enyl-1H-indol-3-yl)-4-(1H-indol-3-yl)-pyrrole-2,5-dione

Guidance literature:: Multi-step reaction with 2 steps

1.1: EtMgBr / tetrahydrofuran; diethyl ether; toluene / Heating

1.2: 67 percent / tetrahydrofuran; diethyl ether; toluene / Heating

2.1: Cs₂CO₃; Bu₄NI / dimethylformamide / 1 h / 23 °C

2.2: 36 percent / dimethylformamide / 96 h / 52 °C

With ethylmagnesium bromide; tetra-(n-butyl)ammonium iodide; caesium carbonate; In tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide; toluene;
DOI:10.1039/b405010j