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Technology Process of (1R,2R)-N1-[{(tert-butylamino)dimethylsilyl}methyl]-N1,N2,N2-trimethylcyclohexane-1,2-diamine

(1R,2R)-N1-[{(tert-butylamino)dimethylsilyl}methyl]-N1,N2,N2-trimethylcyclohexane-1,2-diamine

Base Information
  • Chemical Name:(1R,2R)-N1-[{(tert-butylamino)dimethylsilyl}methyl]-N1,N2,N2-trimethylcyclohexane-1,2-diamine
  • CAS No.:1356406-52-4
  • Molecular Formula:C16H37N3Si
  • Molecular Weight:299.575
  • Hs Code.:
(1R,2R)-N<sub>1</sub>-[{(tert-butylamino)dimethylsilyl}methyl]-N<sub>1</sub>,N<sub>2</sub>,N<sub>2</sub>-trimethylcyclohexane-1,2-diamine

Synonyms:(1R,2R)-N1-[{(tert-butylamino)dimethylsilyl}methyl]-N1,N2,N2-trimethylcyclohexane-1,2-diamine

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Chemical Property of (1R,2R)-N1-[{(tert-butylamino)dimethylsilyl}methyl]-N1,N2,N2-trimethylcyclohexane-1,2-diamine
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Technology Process of (1R,2R)-N1-[{(tert-butylamino)dimethylsilyl}methyl]-N1,N2,N2-trimethylcyclohexane-1,2-diamine

There total 1 articles about (1R,2R)-N1-[{(tert-butylamino)dimethylsilyl}methyl]-N1,N2,N2-trimethylcyclohexane-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

dimethyldimethoxysilan
1112-39-6

dimethyldimethoxysilan

(1R,2R)-bis(dimethylamino)cyclohexane
38383-49-2,43148-65-8,46026-77-1,53100-04-2,53152-68-4,53152-69-5

(1R,2R)-bis(dimethylamino)cyclohexane

lithium tert-butylamide
37828-54-9

lithium tert-butylamide

(1R,2R)-N<sub>1</sub>-[{(tert-butylamino)dimethylsilyl}methyl]-N<sub>1</sub>,N<sub>2</sub>,N<sub>2</sub>-trimethylcyclohexane-1,2-diamine
1356406-52-4

(1R,2R)-N1-[{(tert-butylamino)dimethylsilyl}methyl]-N1,N2,N2-trimethylcyclohexane-1,2-diamine

Guidance literature:
(1R,2R)-bis(dimethylamino)cyclohexane; With n-butyllithium; In pentane; at -80 - 20 ℃; for 4h;
dimethyldimethoxysilan; In pentane; at 0 - 20 ℃; for 1h;
lithium tert-butylamide; In hexane; pentane; at 0 - 20 ℃; for 1h;
DOI:10.1039/c1dt11550b
upstream raw materials:

dimethyldimethoxysilan

(1R,2R)-bis(dimethylamino)cyclohexane

lithium tert-butylamide

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