4-(5-(4-(N-phenyl-N-(4-methoxy)phenylamino)phenyl)thienyl-2)-7-bromo-2,1,3-benzothiadiazole

Base Information

• Chemical Name: 4-(5-(4-(N-phenyl-N-(4-methoxy)phenylamino)phenyl)thienyl-2)-7-bromo-2,1,3-benzothiadiazole
• CAS No.: 1004510-85-3
• Molecular Formula: C₂₉H₂₀BrN₃OS₂
• Molecular Weight: 570.533

Synonyms:4-(5-(4-(N-phenyl-N-(4-methoxy)phenylamino)phenyl)thienyl-2)-7-bromo-2,1,3-benzothiadiazole

Chemical Property of 4-(5-(4-(N-phenyl-N-(4-methoxy)phenylamino)phenyl)thienyl-2)-7-bromo-2,1,3-benzothiadiazole

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Technology Process of 4-(5-(4-(N-phenyl-N-(4-methoxy)phenylamino)phenyl)thienyl-2)-7-bromo-2,1,3-benzothiadiazole

There total 1 articles about 4-(5-(4-(N-phenyl-N-(4-methoxy)phenylamino)phenyl)thienyl-2)-7-bromo-2,1,3-benzothiadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

4,7-dibromobenzo[c][1,2,5]thiadiazole (15155-41-6) + tributyl(5-(4-(N-phenyl-N-(4-methoxy)phenylamino)phenyl)thienyl-2)stannane (1004510-84-2) → 4-(5-(4-(N-phenyl-N-(4-methoxy)phenylamino)phenyl)thienyl-2)-7-bromo-2,1,3-benzothiadiazole (1004510-85-3)

Guidance literature:

tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; at 100 ℃; for 24h;

DOI:10.1039/b712562c

Reference yield: 86.0%

4-(5-(4-(N-phenyl-N-(4-methoxy)phenylamino)phenyl)thienyl-2)-7-bromo-2,1,3-benzothiadiazole (1004510-85-3) + N,N-diphenyl-4-(5-(tributylbutylstannyl)thiophen-2-yl)aniline → 4-(5-(4-(N-phenyl-N-(4-methoxy)phenylamino)phenyl)thienyl-2)-7-(5-(4-(diphenylamino)phenyl)thienyl-2)-2,1,3-benzothiadiazole (1004510-87-5)

Guidance literature:

tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; at 100 ℃; for 24h;

DOI:10.1039/b712562c

Reference yield: 78.0%

4-(5-(4-(N-phenyl-N-(4-methoxy)phenylamino)phenyl)thienyl-2)-7-bromo-2,1,3-benzothiadiazole (1004510-85-3) + diphenyl-(4-tributylstannanyl-phenyl)-amine → 4-(5-(4-(N-phenyl-N-(4-methoxy)phenylamino)phenyl)thienyl-2)-7-(4-(diphenylamino)phenyl)-2,1,3-benzothiadiazole (1004510-86-4)

Guidance literature:

tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; at 100 ℃; for 24h;

DOI:10.1039/b712562c

upstream raw materials:

4,7-dibromobenzo[c][1,2,5]thiadiazole

tributyl(5-(4-(N-phenyl-N-(4-methoxy)phenylamino)phenyl)thienyl-2)stannane

Downstream raw materials:

4-(5-(4-(N-phenyl-N-(4-methoxy)phenylamino)phenyl)thienyl-2)-7-(4-(diphenylamino)phenyl)-2,1,3-benzothiadiazole

4-(5-(4-(N-phenyl-N-(4-methoxy)phenylamino)phenyl)thienyl-2)-7-(5-(4-(diphenylamino)phenyl)thienyl-2)-2,1,3-benzothiadiazole

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