diphenylmethyl 7-phenylacetylamino-3-hydroxy-3-(2-methylprop-2-enyl)cepham-4-carboxylate

Base Information

Chemical Name:diphenylmethyl 7-phenylacetylamino-3-hydroxy-3-(2-methylprop-2-enyl)cepham-4-carboxylate
CAS No.:315206-87-2
Molecular Formula:C₃₂H₃₂N₂O₅S
Molecular Weight:556.682
Hs Code.:

Synonyms:diphenylmethyl 7-phenylacetylamino-3-hydroxy-3-(2-methylprop-2-enyl)cepham-4-carboxylate

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Chemical Property of diphenylmethyl 7-phenylacetylamino-3-hydroxy-3-(2-methylprop-2-enyl)cepham-4-carboxylate

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Technology Process of diphenylmethyl 7-phenylacetylamino-3-hydroxy-3-(2-methylprop-2-enyl)cepham-4-carboxylate

There total 1 articles about diphenylmethyl 7-phenylacetylamino-3-hydroxy-3-(2-methylprop-2-enyl)cepham-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1458-98-6
2-methyl-3-bromo-1-propene

: 54639-48-4
(6R,7R)-benzhydryl 3-hydroxy-8-oxo-7-(2-phenylacetamido)-5-thia-1-azabicyclo[4.2.0]oct-2-ene-2-carboxylate

: 315206-87-2
diphenylmethyl 7-phenylacetylamino-3-hydroxy-3-(2-methylprop-2-enyl)cepham-4-carboxylate

Guidance literature:: With indium; In tetrahydrofuran; water; at 60 ℃; for 24h;
DOI:10.1080/00397910008087052

Reference yield:

: 108-24-7
acetic anhydride

: 315206-87-2
diphenylmethyl 7-phenylacetylamino-3-hydroxy-3-(2-methylprop-2-enyl)cepham-4-carboxylate

: (2R,3R,6R,7R)-3-Acetoxy-3-(2-methyl-allyl)-8-oxo-7-phenylacetylamino-5-thia-1-aza-bicyclo[4.2.0]octane-2-carboxylic acid benzhydryl ester

Guidance literature:: With dmap; In pyridine; at 50 - 60 ℃;
DOI:10.1080/00397910008087052

Reference yield:

: 315206-87-2
diphenylmethyl 7-phenylacetylamino-3-hydroxy-3-(2-methylprop-2-enyl)cepham-4-carboxylate

: (2R,3R,6R,7R)-3-Acetoxy-3-(2-methyl-allyl)-5,8-dioxo-7-phenylacetylamino-5λ⁴-thia-1-aza-bicyclo[4.2.0]octane-2-carboxylic acid benzhydryl ester

Guidance literature:: Multi-step reaction with 2 steps

1: DMAP / pyridine / 50 - 60 °C

2: mCPBA / CH₂Cl₂ / 0 °C

With dmap; 3-chloro-benzenecarboperoxoic acid; In pyridine; dichloromethane; 1: Acetylation / 2: Oxidation;
DOI:10.1080/00397910008087052