methyl (p-tolyl 4,7,8,9-tetra-O-acetyl-3,5-dideoxy-2-thio-5-trichloroacetamido-D-glycero-D-galacto-2-nonulopyranosyl)onate

Base Information

Chemical Name:methyl (p-tolyl 4,7,8,9-tetra-O-acetyl-3,5-dideoxy-2-thio-5-trichloroacetamido-D-glycero-D-galacto-2-nonulopyranosyl)onate
CAS No.:1071226-28-2
Molecular Formula:C₂₇H₃₂Cl₃NO₁₂S
Molecular Weight:700.976
Hs Code.:

Synonyms:methyl (p-tolyl 4,7,8,9-tetra-O-acetyl-3,5-dideoxy-2-thio-5-trichloroacetamido-D-glycero-D-galacto-2-nonulopyranosyl)onate

Suppliers and Price of methyl (p-tolyl 4,7,8,9-tetra-O-acetyl-3,5-dideoxy-2-thio-5-trichloroacetamido-D-glycero-D-galacto-2-nonulopyranosyl)onate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of methyl (p-tolyl 4,7,8,9-tetra-O-acetyl-3,5-dideoxy-2-thio-5-trichloroacetamido-D-glycero-D-galacto-2-nonulopyranosyl)onate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl (p-tolyl 4,7,8,9-tetra-O-acetyl-3,5-dideoxy-2-thio-5-trichloroacetamido-D-glycero-D-galacto-2-nonulopyranosyl)onate

There total 1 articles about methyl (p-tolyl 4,7,8,9-tetra-O-acetyl-3,5-dideoxy-2-thio-5-trichloroacetamido-D-glycero-D-galacto-2-nonulopyranosyl)onate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 598-99-2
Methyl trichloroacetate

: 1071226-27-1
methyl (2-p-methylphenyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α/β-D-galacto-2-thio-nonulopyranosid)onate

: 108-24-7
acetic anhydride

: 1071226-28-2
methyl (p-tolyl 4,7,8,9-tetra-O-acetyl-3,5-dideoxy-2-thio-5-trichloroacetamido-D-glycero-D-galacto-2-nonulopyranosyl)onate

Guidance literature:: methyl (2-p-methylphenyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α/β-D-galacto-2-thio-nonulopyranosid)onate; With methanesulfonic acid; In methanol; at 60 ℃; for 24h;

Methyl trichloroacetate; With triethylamine; In methanol; at 20 ℃; for 6h;

acetic anhydride; With pyridine; dmap; at 0 - 20 ℃;
DOI:10.1002/chem.200800757

Reference yield: 27.0%

: 1071226-28-2
methyl (p-tolyl 4,7,8,9-tetra-O-acetyl-3,5-dideoxy-2-thio-5-trichloroacetamido-D-glycero-D-galacto-2-nonulopyranosyl)onate

: 338744-49-3
3-azidopropyl (2,6-di-O-benzyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

: 1360862-24-3
C₇₀H₈₁Cl₃N₄O₂₃

Guidance literature:: With p-methylbenzenesulfenyl chloride; silver trifluoromethanesulfonate; In dichloromethane; acetonitrile; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1007/s11426-011-4449-x