2-benzyloxymethyl-2-[4-(2-tetrahydropyranyloxy)butyl]-1,3-cyclohexanedione

Base Information

Chemical Name:2-benzyloxymethyl-2-[4-(2-tetrahydropyranyloxy)butyl]-1,3-cyclohexanedione
CAS No.:949587-22-8
Molecular Formula:C₂₃H₃₂O₅
Molecular Weight:388.504
Hs Code.:

Synonyms:2-benzyloxymethyl-2-[4-(2-tetrahydropyranyloxy)butyl]-1,3-cyclohexanedione

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Chemical Property of 2-benzyloxymethyl-2-[4-(2-tetrahydropyranyloxy)butyl]-1,3-cyclohexanedione

Chemical Property:

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Technology Process of 2-benzyloxymethyl-2-[4-(2-tetrahydropyranyloxy)butyl]-1,3-cyclohexanedione

There total 4 articles about 2-benzyloxymethyl-2-[4-(2-tetrahydropyranyloxy)butyl]-1,3-cyclohexanedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-[4-(1-benzyloxymethyl-2,6-dimethoxycyclohexa-2,5-dienyl)butoxy]tetrahydropyran

: 949587-22-8
2-benzyloxymethyl-2-[4-(2-tetrahydropyranyloxy)butyl]-1,3-cyclohexanedione

Guidance literature:: With hydrogenchloride; In acetone; at 20 ℃; for 5h;
DOI:10.1021/jo0709100

Reference yield:

: 949587-21-7
2,6-dimethoxy-1-[4-(2-tetrahydropyranyloxy)butyl]cyclohexa-2,5-dienecarboxylic acid methyl ester

: 949587-22-8
2-benzyloxymethyl-2-[4-(2-tetrahydropyranyloxy)butyl]-1,3-cyclohexanedione

Guidance literature:: Multi-step reaction with 3 steps

1: DIBAL-H / CH₂Cl₂ / 2 h / -78 °C

2: NaH; tetrabutyl ammonium iodide / dimethylformamide / 48 h / 20 °C

3: 193 mg / aq. HCl / acetone / 5 h / 20 °C

With hydrogenchloride; tetra-(n-butyl)ammonium iodide; sodium hydride; diisobutylaluminium hydride; In dichloromethane; N,N-dimethyl-formamide; acetone;
DOI:10.1021/jo0709100

Reference yield:

: [2,6-dimethoxy-1-[4-(2-tetrahydropyranyloxy)butyl]cyclohexa-2,5-dienyl]methanol

: 949587-22-8
2-benzyloxymethyl-2-[4-(2-tetrahydropyranyloxy)butyl]-1,3-cyclohexanedione

Guidance literature:: Multi-step reaction with 2 steps

1: NaH; tetrabutyl ammonium iodide / dimethylformamide / 48 h / 20 °C

2: 193 mg / aq. HCl / acetone / 5 h / 20 °C

With hydrogenchloride; tetra-(n-butyl)ammonium iodide; sodium hydride; In N,N-dimethyl-formamide; acetone;
DOI:10.1021/jo0709100