C₂₈H₃₆O₄

Base Information

Chemical Name:C₂₈H₃₆O₄
CAS No.:897041-95-1
Molecular Formula:C₂₈H₃₆O₄
Molecular Weight:436.591
Hs Code.:

C<sub>28</sub>H<sub>36</sub>O<sub>4</sub>

Synonyms:C₂₈H₃₆O₄

Suppliers and Price of C₂₈H₃₆O₄

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₈H₃₆O₄

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₈H₃₆O₄

There total 13 articles about C₂₈H₃₆O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 897041-93-9
(R)-4-Isopropyl-2-[(2R,6S,8aS)-2-(4-methoxy-phenyl)-6-methyl-6-vinyl-6,7,8,8a-tetrahydro-4H-benzo[1,3]dioxin-5-ylmethyl]-3-methyl-cyclopent-2-enone

: 897041-95-1
C₂₈H₃₆O₄

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In diethyl ether; for 3h; Heating;
DOI:10.1021/ja060847g

Reference yield:

: (1R,4R)-1-Methyl-5-oxo-bicyclo[2.2.2]oct-2-ene-2,3-dicarboxylic acid dimethyl ester

: 897041-95-1
C₂₈H₃₆O₄

Guidance literature:: Multi-step reaction with 11 steps

1.1: 96 percent / mCPBA; NaHCO₃ / CH₂Cl₂ / 12 h / 20 °C

2.1: 100 percent / camphorsulfonic acid / 16 h / Heating

3.1: 84 percent / camphorsulfonic acid / CH₂Cl₂ / 36 h

4.1: 65 percent / lithium aluminum hydride / diethyl ether / 5 h / 0 - 20 °C

5.1: 80 percent / pyridinium p-toluenesulfonic acid / CH₂Cl₂ / 19 h

6.1: o-nitrophenylselenocyanate; tri-n-butylphosphine / tetrahydrofuran / 1 h / 0 °C

6.2: 71 percent / aq. H₂O₂ / tetrahydrofuran / 3 h / 0 - 45 °C

7.1: 82 percent / pyridinium p-toluenesulfonic acid / methanol / 2 h

8.1: 69 percent / DDQ / CH₂Cl₂ / 0.5 h / 20 °C

9.1: N,N-dimethylaminopyridine; dicyclohexylacarbodiimide / CH₂Cl₂ / 1.5 h / 0 - 20 °C

10.1: 78 percent / tetrakis(triphenylphosphine)palladium; LiCl; cuprous chloride / dimethylsulfoxide / 18 h / 20 - 60 °C

11.1: 82 percent / diisopropylethylamine / diethyl ether / 3 h / Heating

With dmap; lithium aluminium tetrahydride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; ortho-nitrophenyl selenocyanate; tributylphosphine; camphor-10-sulfonic acid; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; dicyclohexyl-carbodiimide; 2,3-dicyano-5,6-dichloro-p-benzoquinone; copper(l) chloride; lithium chloride; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; dimethyl sulfoxide;
DOI:10.1021/ja060847g

Reference yield:

: (1R,5R)-5-Methyl-3-oxo-2-oxa-bicyclo[3.2.2]non-6-ene-6,7-dicarboxylic acid dimethyl ester

: 897041-95-1
C₂₈H₃₆O₄

Guidance literature:: Multi-step reaction with 10 steps

1.1: 100 percent / camphorsulfonic acid / 16 h / Heating

2.1: 84 percent / camphorsulfonic acid / CH₂Cl₂ / 36 h

3.1: 65 percent / lithium aluminum hydride / diethyl ether / 5 h / 0 - 20 °C

4.1: 80 percent / pyridinium p-toluenesulfonic acid / CH₂Cl₂ / 19 h

5.1: o-nitrophenylselenocyanate; tri-n-butylphosphine / tetrahydrofuran / 1 h / 0 °C

5.2: 71 percent / aq. H₂O₂ / tetrahydrofuran / 3 h / 0 - 45 °C

6.1: 82 percent / pyridinium p-toluenesulfonic acid / methanol / 2 h

7.1: 69 percent / DDQ / CH₂Cl₂ / 0.5 h / 20 °C

8.1: N,N-dimethylaminopyridine; dicyclohexylacarbodiimide / CH₂Cl₂ / 1.5 h / 0 - 20 °C

9.1: 78 percent / tetrakis(triphenylphosphine)palladium; LiCl; cuprous chloride / dimethylsulfoxide / 18 h / 20 - 60 °C

10.1: 82 percent / diisopropylethylamine / diethyl ether / 3 h / Heating

With dmap; lithium aluminium tetrahydride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; ortho-nitrophenyl selenocyanate; tributylphosphine; camphor-10-sulfonic acid; pyridinium p-toluenesulfonate; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; 2,3-dicyano-5,6-dichloro-p-benzoquinone; copper(l) chloride; lithium chloride; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; dimethyl sulfoxide;
DOI:10.1021/ja060847g