(-)-(1R,2R,5R)-2-azido-6-benzyl-8-(4-methoxybenzyl)-6,8-diazabicyclo[3.2.2]nonane-7,9-dione

Base Information

• Chemical Name: (-)-(1R,2R,5R)-2-azido-6-benzyl-8-(4-methoxybenzyl)-6,8-diazabicyclo[3.2.2]nonane-7,9-dione
• CAS No.: 1228313-35-6
• Molecular Formula: C₂₂H₂₃N₅O₃
• Molecular Weight: 405.456

Synonyms:(-)-(1R,2R,5R)-2-azido-6-benzyl-8-(4-methoxybenzyl)-6,8-diazabicyclo[3.2.2]nonane-7,9-dione

Chemical Property of (-)-(1R,2R,5R)-2-azido-6-benzyl-8-(4-methoxybenzyl)-6,8-diazabicyclo[3.2.2]nonane-7,9-dione

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Technology Process of (-)-(1R,2R,5R)-2-azido-6-benzyl-8-(4-methoxybenzyl)-6,8-diazabicyclo[3.2.2]nonane-7,9-dione

There total 2 articles about (-)-(1R,2R,5R)-2-azido-6-benzyl-8-(4-methoxybenzyl)-6,8-diazabicyclo[3.2.2]nonane-7,9-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

(-)-(1R,2S,5R)-6-benzyl-2-hydroxy-8-(4-methoxybenzyl)-6,8-diazabicyclo[3.2.2]nonane-7,9-dione (960599-46-6) → (-)-(1R,2R,5R)-2-azido-6-benzyl-8-(4-methoxybenzyl)-6,8-diazabicyclo[3.2.2]nonane-7,9-dione (1228313-35-6)

Guidance literature:

With hydrogen azide; di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; benzene; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1021/jm100182p

Reference yield:

C23H26N2O6S (1190955-67-9) → (-)-(1R,2R,5R)-2-azido-6-benzyl-8-(4-methoxybenzyl)-6,8-diazabicyclo[3.2.2]nonane-7,9-dione (1228313-35-6)

Guidance literature:

With sodium azide; In N,N-dimethyl-formamide; at 130 ℃; for 18h; Inert atmosphere;

DOI:10.1021/jm100182p

Reference yield:

(-)-(1R,2R,5R)-2-azido-6-benzyl-8-(4-methoxybenzyl)-6,8-diazabicyclo[3.2.2]nonane-7,9-dione (1228313-35-6) → (1R,2R,5R)-2-amino-6-benzyl-8-(4-methoxybenzyl)-6,8-diazabicyclo[3.2.2]nonane-7,9-dione (1228313-38-9)

Guidance literature:

With palladium 10% on activated carbon; ammonium formate; In methanol; for 2h; Reflux;

DOI:10.1021/jm100182p

upstream raw materials:

(-)-(1R,2S,5R)-6-benzyl-2-hydroxy-8-(4-methoxybenzyl)-6,8-diazabicyclo[3.2.2]nonane-7,9-dione

C₂₃H₂₆N₂O₆S

Downstream raw materials:

(1R,2R,5R)-2-amino-6-benzyl-8-(4-methoxybenzyl)-6,8-diazabicyclo[3.2.2]nonane-7,9-dione

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